Technology Process of Imidodisulfurylchloride
There total 12 articles about Imidodisulfurylchloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
thionyl chloride;
amidosulfuric acid placed into a flask and suspended in thionyl dichloride under dry N2; HSO3Cl added, then the flask fitted with a reflux condenser, connected to a CaCl2 drying tube; heated at 130°C for 24 h; reaction mixture fractionally distilled under vacuum; main fraction collected at 95°C/650 Pa;
DOI:10.1002/zaac.200400325
- Guidance literature:
-
With
chlorosulfonic acid;
at 130 ℃;
for 24h;
Inert atmosphere;
- Guidance literature:
-
at 70 - 130 ℃;
for 24h;