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Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-

Base Information Edit
  • Chemical Name:Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-
  • CAS No.:139356-38-0
  • Molecular Formula:C20H41ClO2Si2
  • Molecular Weight:405.168
  • Hs Code.:
  • DSSTox Substance ID:DTXSID201112585
  • Mol file:139356-38-0.mol
Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-

Synonyms:139356-38-0;Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-;tert-butyl-[(1R,3R)-3-[tert-butyl(dimethyl)silyl]oxy-5-(2-chloroethylidene)cyclohexyl]oxy-dimethylsilane;Paricalcitol Impurity B01;(((1R,3R)-5-(2-chloroethylidene)cyclohexane-1,3-diyl)bis(oxy)) bis(tert-butyldimethylsilane);DTXSID201112585

Suppliers and Price of Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 3 raw suppliers
Chemical Property of Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl- Edit
Chemical Property:
  • Hydrogen Bond Donor Count:0
  • Hydrogen Bond Acceptor Count:2
  • Rotatable Bond Count:7
  • Exact Mass:404.2333613
  • Heavy Atom Count:25
  • Complexity:435
Purity/Quality:

NLT 98% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
  • Canonical SMILES:CC(C)(C)[Si](C)(C)OC1CC(CC(=CCCl)C1)O[Si](C)(C)C(C)(C)C
  • Isomeric SMILES:CC(C)(C)[Si](C)(C)O[C@H]1C[C@@H](CC(=CCCl)C1)O[Si](C)(C)C(C)(C)C
Technology Process of Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl-

There total 25 articles about Silane, [[(1R,3R)-5-(2-chloroethylidene)-1,3-cyclohexanediyl]bis(oxy)]bis[(1,1-dimethylethyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 86 percent / LDA / tetrahydrofuran / 2 h / -78 °C
2: DIBAL-H / toluene / 1 h / -78 °C
3: 80 percent / N-chlorosuccinimide-dimethylsulfide complex / CH2Cl2 / -25 - 0 °C
With N-chlorosuccinimide-dimethylsulfide; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/0040-4039(91)80559-O
Guidance literature:
Multi-step reaction with 4 steps
1: 78 percent / satd. NaIO4 / H2O; methanol / 0.5 h / 0 °C
2: 86 percent / LDA / tetrahydrofuran / 2 h / -78 °C
3: DIBAL-H / toluene / 1 h / -78 °C
4: 80 percent / N-chlorosuccinimide-dimethylsulfide complex / CH2Cl2 / -25 - 0 °C
With sodium periodate; N-chlorosuccinimide-dimethylsulfide; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1016/0040-4039(91)80559-O
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