erythro-Pentitol,3-amino-1,4-anhydro-2,3,5-trideoxy-(9CI)

Base Information

• Chemical Name: erythro-Pentitol,3-amino-1,4-anhydro-2,3,5-trideoxy-(9CI)
• CAS No.: 149420-97-3
• Molecular Formula: C₅H₁₁NO
• Molecular Weight: 101.148
• Mol file: 149420-97-3.mol

Synonyms:3-Furanamine,tetrahydro-2-methyl-, trans-

Chemical Property of erythro-Pentitol,3-amino-1,4-anhydro-2,3,5-trideoxy-(9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of erythro-Pentitol,3-amino-1,4-anhydro-2,3,5-trideoxy-(9CI)

There total 4 articles about erythro-Pentitol,3-amino-1,4-anhydro-2,3,5-trideoxy-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyltetrahydrofuran-3-one (3188-00-9) → trans-2-METHYL-3-TETRAHYDROFURYLAMINE (149420-97-3,292054-35-4,458566-77-3)

Guidance literature:

In methanol; hydrogen;

Reference yield:

2-methyl-dihydro-furan-3-one oxime → 2-methyltetrahydrofuran-3-amine (149420-97-3,292054-35-4,458566-77-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;

DOI:10.3797/scipharm.aut-00-09

Reference yield:

2-methyltetrahydrofuran-3-one (3188-00-9) → 2-methyltetrahydrofuran-3-amine (149420-97-3,292054-35-4,458566-77-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₂OH*HCl; NaHCO₃ / diethyl ether / 24 h

2: LiAlH₄ / tetrahydrofuran / 2 h / Heating

With lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; 1: Condensation / 2: Reduction;

DOI:10.3797/scipharm.aut-00-09

upstream raw materials:

2-methyltetrahydrofuran-3-one

Refernces

• 1、 -. "Fungicidal heterocyclic aromatic amides and their compositions, methods of use and preparation". . . Retrieved 2008/06/13.