1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan

Base Information

• Chemical Name: 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan
• CAS No.: 57908-47-1
• Molecular Formula: C₂₀H₂₂N₂O₄
• Molecular Weight: 354.406
• Mol file: 57908-47-1.mol

Synonyms:1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan

Chemical Property of 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan

Chemical Property:

• Melting Point: 115 °C(Solv: hexane (110-54-3))
• Boiling Point: 419.4±45.0 °C(Predicted)
• PSA: 77.32000
• Density: 1.10±0.1 g/cm3(Predicted)
• LogP: 4.31060

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan

There total 3 articles about 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoetan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.3%

sodium acetate (127-09-3) + 1,1'-dichloro-1,1'-diphenyl-1,1'-azoethane (19727-23-2) → 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoethan (57908-47-1)

Guidance literature:

With acetic acid; In acetone; for 2h;

DOI:10.1007/BF00808940

Reference yield:

acetophenonazine (729-43-1) → 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoethan (57908-47-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 81.8 percent / liquid Cl₂ / 1 h / -70 °C

2: 67.3 percent / CH₃COOH / acetone / 2 h

With chlorine; acetic acid; In acetone;

DOI:10.1007/BF00808940

Reference yield:

→ 1,1'-Diacetoxy-1,1'-diphenyl-1,1'-azoethan (57908-47-1)

Guidance literature:

1,1'-Dichlor-1,1'-diphenyl-1,1'-azoethan, Silberacetat;

upstream raw materials:

sodium acetate

1,1'-dichloro-1,1'-diphenyl-1,1'-azoethane

acetophenonazine

Refernces