manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine

Base Information

• Chemical Name: manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine
• CAS No.: 133629-42-2
• Molecular Formula: C₅₆H₅₂ClMnN₄O₁₂
• Molecular Weight: 1063.44
• Mol file: 133629-42-2.mol

Synonyms:

Chemical Property of manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine

There total 1 articles about manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.3%

5,10,15,20-tetra(1,2,3-trimethoxyphenyl)-21H,23H-porphine + manganese (II) acetate tetrahydrate (6156-78-1) → manganese(III)Cl(3,4,5-trimethoxyphenyl)4porphyrine (133629-42-2)

Guidance literature:

With air; HCl; In N,N-dimethyl-formamide; addn. of Mn(OAc)2, refluxing until no free-base porphyrine bands were found in the visible spectrum, cooling to room temp., pouring in ice-cooled NaCl soln., washing of the ppt. with water, air drying, dissolving in MeOH, filtn. and pouring into 6 M HCl; filtn., washing with water, air drying, extn. with CH2Cl2, concn., addn. of hexane and drying by infrared; elem. anal.;

upstream raw materials:

manganese (II) acetate tetrahydrate