C₁₃H₁₃N₃O₃

Base Information

• Chemical Name: C₁₃H₁₃N₃O₃
• CAS No.: 1422434-54-5
• Molecular Formula: C₁₃H₁₃N₃O₃
• Molecular Weight: 259.265
• Mol file: 1422434-54-5.mol

Synonyms:

Chemical Property of C₁₃H₁₃N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₃N₃O₃

There total 3 articles about C₁₃H₁₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-6-chloro-3-nitropyridine (27048-04-0) → C13H13N3O3 (1422434-54-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 80 °C

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 0 °C

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1039/c2ob26710a

Reference yield:

methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → C13H13N3O3 (1422434-54-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 80 °C

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 0 °C

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1039/c2ob26710a

Reference yield:

C13H11N3O5 (1422434-51-2) → C13H13N3O3 (1422434-54-5)

Guidance literature:

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; at 0 ℃;

DOI:10.1039/c2ob26710a

upstream raw materials:

2-amino-6-chloro-3-nitropyridine

C₁₃H₁₁N₃O₅

methyl 4-hydroxylbenzoate

Downstream raw materials:

C₂₀H₁₇Cl₂N₃O₃

Refernces