Technology Process of 6-Isopropylpyridine-3-boronic acid pinacol ester
There total 3 articles about 6-Isopropylpyridine-3-boronic acid pinacol ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 15 ℃;
for 16h;
under 775.743 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,4-dioxane / 16 h / 90 °C / Inert atmosphere
2: potassium acetate / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere
3: palladium on activated charcoal; hydrogen / methanol / 16 h / 15 °C / 775.74 Torr
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on activated charcoal; hydrogen; potassium acetate; potassium carbonate;
In
1,4-dioxane; methanol; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium acetate / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere
2: palladium on activated charcoal; hydrogen / methanol / 16 h / 15 °C / 775.74 Torr
With
palladium on activated charcoal; hydrogen; potassium acetate;
In
1,4-dioxane; methanol;