3-(Hydroxymethyl)cyclohexanone

Base Information

• Chemical Name: 3-(Hydroxymethyl)cyclohexanone
• CAS No.: 21996-61-2
• Molecular Formula: C7H12O2
• Molecular Weight: 128.169
• Mol file: 21996-61-2.mol

Synonyms:3-(Hydroxymethyl)cyclohexan-1-one;

Chemical Property of 3-(Hydroxymethyl)cyclohexanone

Chemical Property:

• Vapor Pressure: 0.00688mmHg at 25°C
• Refractive Index: 1.472
• Boiling Point: 239.8 °C at 760 mmHg
• Flash Point: 98 °C
• PSA: 37.30000
• Density: 1.054 g/cm³
• LogP: 0.73800
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3-(Hydroxymethyl)cyclohexanone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(Hydroxymethyl)cyclohexanone

There total 2 articles about 3-(Hydroxymethyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(ethoxymethoxy)methyl]benzene (54673-14-2) + tri-n-butylstannylmethanol (27490-33-1) + 2-((R)-Toluene-4-sulfinyl)-cyclohex-2-enone → (R)-3-Hydroxymethyl-cyclohexanone (21996-61-2) + (S)-3-Hydroxymethyl-cyclohexanone

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

→ (R)-3-Hydroxymethyl-cyclohexanone (21996-61-2)

Guidance literature:

Nitrosamid 13, Δ, Na2CO3;

DOI:10.1021/jo01264a021

upstream raw materials:

[(ethoxymethoxy)methyl]benzene

tri-n-butylstannylmethanol

Refernces