ethylenediaminetetra-3-propionate^(4-)copper(II)

Base Information

• Chemical Name: ethylenediaminetetra-3-propionate^(4-)copper(II)
• CAS No.: 105022-99-9
• Molecular Formula: C₁₄H₂₀CuN₂O₈
• Molecular Weight: 407.867
• Mol file: 105022-99-9.mol

Synonyms:

Chemical Property of ethylenediaminetetra-3-propionate^(4-)copper(II)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethylenediaminetetra-3-propionate^(4-)copper(II)

There total 1 articles about ethylenediaminetetra-3-propionate^(4-)copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloropropionic acid (107-94-8) + copper(II) choride dihydrate + ethylenediamine-N-acetic acid dihydrochloride dihydrate + chloroacetic acid (79-11-8) + magnesium chloride (7786-30-3) → copper(II) ethylenediaminetetraacetate + ethylenediaminetetra-3-propionate(4-)copper(II) (105022-99-9,212628-41-6) + (ethylenediamine-N,N-diacetato-N',N'-di-3-propionato)cuprate(II) + magnesium (ethylenediamine-N,N,N′-triacetate-N′-3-propionate)cuprate(II) octahydrate

Guidance literature:

In water; byproducts: NaCl; gradual condensation of ethylenediamine-N-acetic acid*2HCl*2H2O with theorganic acids in aq. NaOH; pH 5 adjusted by HCl; solid CuCl2*2H2O added , stirred at 40°C for 2 h; adjusted to pH 7 by NaHCO3; stirred at70°C for 2 h; concn.; filtration; chromy. (G-10 Sephadex, water); chromy. (Dowex 1-X8,Cl(-) form; elution with water, then with 0.05M MgCl2); concn.; crystn. on cooling for several days; washed with ethanol and ether; air-dried; recrystn. (water); elem. anal.;

DOI:10.1246/bcsj.73.2283

upstream raw materials:

chloropropionic acid

chloroacetic acid

magnesium chloride

Refernces