Technology Process of Cyclohexanecarbothioic acid, S-ethyl ester
There total 15 articles about Cyclohexanecarbothioic acid, S-ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol;
In
toluene;
at 20 ℃;
for 12h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1039/c1ob05352c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol / toluene / 12 h / 20 °C / Inert atmosphere
With
dmap; copper acetate monohydrate; o-phenylenebis(diphenylphosphine); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tert-butyl alcohol;
In
dichloromethane; toluene;
DOI:10.1039/c1ob05352c
