3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride

Base Information

• Chemical Name: 3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride
• CAS No.: 1071558-72-9
• Molecular Formula: C₂₇H₂₈N₂O₃*ClH
• Molecular Weight: 464.992
• Mol file: 1071558-72-9.mol

Synonyms:

Chemical Property of 3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride

There total 1 articles about 3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) + o-(ethylamino)-p-cresol (42485-84-7) + dimethyl sulfate (77-78-1) → 3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride (1071558-72-9)

Guidance literature:

phthalic anhydride; o-(ethylamino)-p-cresol; In various solvent(s); Heating;

dimethyl sulfate; With sodium hydroxide; In various solvent(s); for 5h; Further stages.; Heating;

DOI:10.1039/b803738h

Reference yield:

3,6-bis(ethylamino)-9-[2-(methoxycarbonyl)phenyl]-xanthylium chloride (1071558-72-9) → C46H42N8O3 (1400890-74-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Reflux

2: methanol / 3 h / Reflux

With hydrazine hydrate; In methanol;

DOI:10.1039/c2dt31316b

upstream raw materials:

phthalic anhydride

o-(ethylamino)-p-cresol

dimethyl sulfate

Downstream raw materials:

C₄₆H₄₂N₈O₃

Refernces