Technology Process of C25H38N2O5S2Si
There total 4 articles about C25H38N2O5S2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH2Cl2 / 3 h
2: p-TsOH / acetonitrile / 1.75 h / Heating
3: DCC, 1-hydroxybenzotriazole hydrate, diisopropylethylamine / tetrahydrofuran / 1.) 0 deg C, 1.5 h, 2.) room temperature, 18 h
With
dmap; toluene-4-sulfonic acid; 1-hydroxybenzotriazol-hydrate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm00401a014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: p-TsOH / acetonitrile / 1.75 h / Heating
2: DCC, 1-hydroxybenzotriazole hydrate, diisopropylethylamine / tetrahydrofuran / 1.) 0 deg C, 1.5 h, 2.) room temperature, 18 h
With
toluene-4-sulfonic acid; 1-hydroxybenzotriazol-hydrate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/jm00401a014
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / H2O; acetone / 24 h
2: 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH2Cl2 / 3 h
3: p-TsOH / acetonitrile / 1.75 h / Heating
4: DCC, 1-hydroxybenzotriazole hydrate, diisopropylethylamine / tetrahydrofuran / 1.) 0 deg C, 1.5 h, 2.) room temperature, 18 h
With
dmap; toluene-4-sulfonic acid; 1-hydroxybenzotriazol-hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/jm00401a014