p-chloronitrosobenzene dimer

Base Information

• Chemical Name: p-chloronitrosobenzene dimer
• CAS No.: 149522-74-7
• Molecular Formula: C₁₂H₈Cl₂N₂O₂
• Molecular Weight: 283.114
• Mol file: 149522-74-7.mol

Synonyms:

Chemical Property of p-chloronitrosobenzene dimer

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-chloronitrosobenzene dimer

There total 9 articles about p-chloronitrosobenzene dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-aniline (106-47-8) → bis-(4-chloro-phenyl)-diazene N,N'-dioxide (110972-79-7,149522-74-7) + 4-chlorobenzonitrile (100-00-5)

Guidance literature:

With dihydrogen peroxide; peroxotungstophosphate; In chloroform; for 2h; Ambient temperature;

DOI:10.1246/cl.1992.289

Reference yield:

4-chloro-aniline (106-47-8) → p-chloronitrosobenzene dimer (149522-74-7,110972-79-7) + 4-chlorobenzonitrile (100-00-5)

Guidance literature:

With dihydrogen peroxide; 34>(3-); In chloroform; for 2h; Ambient temperature;

DOI:10.1021/jo00066a012

Reference yield:

N-(4-chlorophenyl)hydroxylamine (823-86-9) → bis-(4-chloro-phenyl)-diazene N,N'-dioxide (110972-79-7,149522-74-7)

Guidance literature:

With iron(III) chloride; In ethanol;

DOI:10.1016/S0040-4020(01)93607-5

upstream raw materials:

N-(4-chlorophenyl)hydroxylamine

4-chloro-aniline

4-bromo-¹⁵N-nitrosobenzene

1-chloro-4-nitroso-benzene

Downstream raw materials:

1-chloro-4-nitroso-benzene

4,4'-bis(chloro)azoxybenzene

Refernces

• 1、 Knezevic, Anamarija,Medancic, Tina,Milovac, Srdan,Biljan, Ivana,Halasz, Ivan,Vancik, Hrvoj. "Photothermal reactions of nitrosobenzene and halonitrosobenzenes in solid-state". scheme or table. p. 21 - 24. Retrieved 2012/02/15.
• 2、 Sakaue, Shigeki,Sakata, Yasuyuki,Nishiyama, Yutaka,Ishii, Yasutaka. "Oxidation of Aliphatic and Aromatic Amines with Hydrogen Peroxide Catralyzed by Peroxoheteropoly Oxometalates". . p. 289 - 292. Retrieved 2007/10/02.