Technology Process of <2-
ethyl>trimethylammonium iodide
There total 4 articles about <2-ethyl>trimethylammonium iodide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tributyl-amine;
In
N,N-dimethyl-formamide;
for 3h;
DOI:10.1021/jo00334a028
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 48percent HBr / 12 h / Heating
2: tetrabutylammonium bromide / CH2Cl2; H2O / 12 h / Heating
3: 53 percent / lithium aluminum hydride, aluminum chloride / diethyl ether / 8 h / Heating
4: 25 percent / tri-n-butylamine / dimethylformamide / 3 h
With
lithium aluminium tetrahydride; aluminium trichloride; tributyl-amine; tetrabutylammomium bromide; hydrogen bromide;
In
diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00334a028
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammonium bromide / CH2Cl2; H2O / 12 h / Heating
2: 53 percent / lithium aluminum hydride, aluminum chloride / diethyl ether / 8 h / Heating
3: 25 percent / tri-n-butylamine / dimethylformamide / 3 h
With
lithium aluminium tetrahydride; aluminium trichloride; tributyl-amine; tetrabutylammomium bromide;
In
diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00334a028
