C₁₅H₁₇Cl₂N₃OS

Base Information

• Chemical Name: C₁₅H₁₇Cl₂N₃OS
• CAS No.: 1386975-90-1
• Molecular Formula: C₁₅H₁₇Cl₂N₃OS
• Molecular Weight: 358.291
• Mol file: 1386975-90-1.mol

Synonyms:

Chemical Property of C₁₅H₁₇Cl₂N₃OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₇Cl₂N₃OS

There total 7 articles about C₁₅H₁₇Cl₂N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H25Cl2N3O3S → C15H17Cl2N3OS (1386975-90-1)

Guidance literature:

With triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In water; at 20 ℃;

DOI:10.1021/jm300303e

Reference yield:

C20H26Cl2N2O2 → C15H17Cl2N3OS (1386975-90-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / water; acetonitrile / 20 °C

2.1: hydrazine / tetrahydrofuran / 0.5 h / 65 °C / Microwave irradiation

3.1: N,N-dimethyl-formamide / 2 h / 20 °C

3.2: 20 °C

4.1: triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid / water / 20 °C

With triisopropylsilyl trifluoromethanesulfonate; potassium carbonate; trifluoroacetic acid; hydrazine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jm300303e

Reference yield:

tert-butyl 3,5-dichlorobenzyl(3-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino)propyl)carbamate (1386975-94-5) → C15H17Cl2N3OS (1386975-90-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrazine / tetrahydrofuran / 0.5 h / 65 °C / Microwave irradiation

2.1: N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 20 °C

3.1: triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid / water / 20 °C

With triisopropylsilyl trifluoromethanesulfonate; trifluoroacetic acid; hydrazine; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1021/jm300303e

upstream raw materials:

2-thiophene isocyanate

N-(3',5'-dichlorobenzyl)-1,3-diaminopropane

tert-butyl 3,5-dichlorobenzyl(3-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino)propyl)carbamate

3,5-dichlorobenzaldehyde

Refernces