C₂₀H₁₇FO

Base Information

• Chemical Name: C₂₀H₁₇FO
• CAS No.: 1445739-96-7
• Molecular Formula: C₂₀H₁₇FO
• Molecular Weight: 292.353
• Mol file: 1445739-96-7.mol

Synonyms:

Chemical Property of C₂₀H₁₇FO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₁₇FO

There total 4 articles about C₂₀H₁₇FO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) → C20H17FO (1445739-96-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium; iodine / diethyl ether / 1.5 h / Reflux

1.2: Reflux

2.1: acetyl chloride / hexane / 3 h / Inert atmosphere; Reflux

3.1: 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; picoline / 21.14 °C / Inert atmosphere

With picoline; iodine; magnesium; acetyl chloride; 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; In diethyl ether; hexane;

DOI:10.1002/anie.201206113

Reference yield:

(4-fluorophenyl)diphenylmethanol (427-39-4) → C20H17FO (1445739-96-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetyl chloride / hexane / 3 h / Inert atmosphere; Reflux

2: 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; picoline / 21.14 °C / Inert atmosphere

With picoline; acetyl chloride; 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; In hexane;

DOI:10.1002/anie.201206113

Reference yield:

1-Bromo-4-fluorobenzene (460-00-4) → C20H17FO (1445739-96-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium; iodine / diethyl ether / 1.5 h / Reflux

1.2: Reflux

2.1: acetyl chloride / hexane / 3 h / Inert atmosphere; Reflux

3.1: 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; picoline / 21.14 °C / Inert atmosphere

With picoline; iodine; magnesium; acetyl chloride; 1-decyl-3-methylimidazolium bis-trifluormethanesulfonimide; In diethyl ether; hexane;

DOI:10.1002/anie.201206113

upstream raw materials:

(4-fluorophenyl)diphenylmethanol

methanol

p-fluorophenyldiphenylmethyl chloride

1-Bromo-4-fluorobenzene

Refernces

• 1、 Weber, Cameron C.,Masters, Anthony F.,Maschmeyer, Thomas. "Pseudo-encapsulation-nanodomains for enhanced reactivity in ionic liquids". . p. 11483 - 11486. Retrieved 2013/01/15.