rengyoxide dimethyl ketal diacetate

Base Information

• Chemical Name: rengyoxide dimethyl ketal diacetate
• CAS No.: 93697-55-3
• Molecular Formula: C₁₄H₂₄O₆
• Molecular Weight: 288.341
• Mol file: 93697-55-3.mol

Synonyms:

Chemical Property of rengyoxide dimethyl ketal diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rengyoxide dimethyl ketal diacetate

There total 5 articles about rengyoxide dimethyl ketal diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rengyol monoacetate (93675-93-5) → rengyoxide dimethyl ketal diacetate (93697-55-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 39 mg / Collins reagens / CH₂Cl₂ / Ambient temperature

2: 5 percent sodium hydroxide / H₂O; methanol

3: 15 mg / 5 percent hydrogen chloride / Ambient temperature

4: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; Collins oxidation agent; In methanol; dichloromethane; water; triethylamine;

DOI:10.1139/v84-343

Reference yield:

rengyol (93675-85-5,101489-38-7) → rengyoxide dimethyl ketal diacetate (93697-55-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 171 mg / ethanol; pyridine / 48 h / Ambient temperature

2: 39 mg / Collins reagens / CH₂Cl₂ / Ambient temperature

3: 5 percent sodium hydroxide / H₂O; methanol

4: 15 mg / 5 percent hydrogen chloride / Ambient temperature

5: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; Collins oxidation agent; In pyridine; methanol; ethanol; dichloromethane; water; triethylamine;

DOI:10.1139/v84-343

Reference yield:

rengyoxide (93675-86-6) → rengyoxide dimethyl ketal diacetate (93697-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 15 mg / 5 percent hydrogen chloride / Ambient temperature

2: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; In triethylamine;

DOI:10.1139/v84-343

upstream raw materials:

acetic anhydride

rengyoxide dimethyl ketal

rengyol monoacetate

rengyol

Refernces