Ph₂PCH₂N(H)C₅H₃(OPPh₂)N

Base Information

• Chemical Name: Ph₂PCH₂N(H)C₅H₃(OPPh₂)N
• CAS No.: 304000-69-9
• Molecular Formula: C₃₀H₂₆N₂OP₂
• Molecular Weight: 492.497
• Mol file: 304000-69-9.mol

Synonyms:

Chemical Property of Ph₂PCH₂N(H)C₅H₃(OPPh₂)N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ph₂PCH₂N(H)C₅H₃(OPPh₂)N

There total 3 articles about Ph₂PCH₂N(H)C₅H₃(OPPh₂)N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) + Ph2PCH2N(H)C5H3(OH)N (304000-63-3) → Ph2PCH2N(H)C5H3(OPPh2)N (304000-69-9)

Guidance literature:

In toluene; at 20 ℃; for 24h; Title compound not separated from byproducts.;

DOI:10.1039/b003759l

Reference yield:

2-amino-3-hydroxypyridine (16867-03-1) → Ph2PCH2N(H)C5H3(OPPh2)N (304000-69-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / methanol; toluene / 24 h / Heating

2: toluene / 24 h / 20 °C

In methanol; toluene; 1: Substitution / 2: Substitution;

DOI:10.1039/b003759l

Reference yield:

diphenylphosphinomethanol (5958-44-1) → Ph2PCH2N(H)C5H3(OPPh2)N (304000-69-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / methanol; toluene / 24 h / Heating

2: toluene / 24 h / 20 °C

In methanol; toluene; 1: Substitution / 2: Substitution;

DOI:10.1039/b003759l

upstream raw materials:

chloro-diphenylphosphine

Ph₂PCH₂N(H)C₅H₃(OH)N

2-amino-3-hydroxypyridine

diphenylphosphinomethanol

Downstream raw materials:

[(RuCl2(η6-p-cymene))2(Ph2PCH2N(H)C5H3(OPPh2)N)]

cis-[PtCl₂(Ph₂PCH₂N(H)C₅H₃(OPPh₂)N)]

[(RuCl2(η6-C6Me6))2(Ph2PCH2N(H)C5H3(OPPh2)N)]

[(IrCl2(η5-C5Me5))2(Ph2PCH2N(H)C5H3(OPPh2)N)]

Refernces