C₃₀H₄₀N₂

Base Information

• Chemical Name: C₃₀H₄₀N₂
• CAS No.: 1271736-32-3
• Molecular Formula: C₃₀H₄₀N₂
• Molecular Weight: 428.661
• Mol file: 1271736-32-3.mol

Synonyms:

Chemical Property of C₃₀H₄₀N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₀N₂

There total 12 articles about C₃₀H₄₀N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2,4,6-trimethylcyclohex-3-ene-1-carbaldehyde (1423-46-7) + cis/trans-N,N'-dibenzylcyclohexane-1,2-diamine (135613-88-6,143443-23-6,65838-10-0,191480-61-2) → C30H40N2 (1271736-32-3)

Guidance literature:

With calcium chloride; In ethanol; water; at 20 ℃; for 120h;

DOI:10.1002/ejoc.201001433

Reference yield:

1,3-dibenzyl-2-phenyl-octahydro-1H-benzimidazole → C30H40N2 (1271736-32-3)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrahydrofuran-d8 / 600 h / phosphate buffer in D₂O

2: methanol / 65 - 70 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

4: calcium chloride / ethanol; water / 120 h / 20 °C

With sodium tetrahydroborate; calcium chloride; In methanol; tetrahydrofuran-d8; ethanol; water;

DOI:10.1002/ejoc.201001433

Reference yield:

(±)-trans-N,N'-dibenzylcyclohexane-1,2-diamine (191480-61-2) → C30H40N2 (1271736-32-3)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrahydrofuran-d8 / 696 h / phosphate buffer in D₂O

2: tetrahydrofuran-d8 / 600 h / phosphate buffer in D₂O

3: methanol / 65 - 70 °C / Inert atmosphere

4: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

5: calcium chloride / ethanol; water / 120 h / 20 °C

With sodium tetrahydroborate; calcium chloride; In methanol; tetrahydrofuran-d8; ethanol; water;

DOI:10.1002/ejoc.201001433

upstream raw materials:

N,N'-(cyclohexane-1,2-diyl)bis(1-phenylmethanimine)

(±)-trans-N,N'-dibenzylcyclohexane-1,2-diamine

N,N'-bisbenzylidene-1,3-diaminopropane

(+/-)-2,4,6-trimethylcyclohex-3-ene-1-carbaldehyde

Refernces