Technology Process of C17H15NO4
There total 5 articles about C17H15NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate;
In
1,2-dimethoxyethane;
at 60 ℃;
for 22h;
optical yield given as %de;
DOI:10.1002/adsc.201100627
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 - 20 °C / Inert atmosphere
1.2: 1.5 h / 20 °C
2.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate / 1,2-dimethoxyethane / 22 h / 60 °C
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tert.-butyl lithium; caesium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; pentane;
DOI:10.1002/adsc.201100627
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -22 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -22 °C / Inert atmosphere
2.2: -78 - 20 °C
3.1: water; iodine; calcium carbonate / tetrahydrofuran / 1.5 h / 20 °C
4.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 - 20 °C / Inert atmosphere
4.2: 1.5 h / 20 °C
5.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate / 1,2-dimethoxyethane / 22 h / 60 °C
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; n-butyllithium; water; iodine; tert.-butyl lithium; caesium carbonate; calcium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane; pentane;
DOI:10.1002/adsc.201100627