(2-chlorobenzyl)ferrocene

Base Information

• Chemical Name: (2-chlorobenzyl)ferrocene
• CAS No.: 287180-12-5
• Molecular Formula: C₁₇H₁₅ClFe
• Molecular Weight: 310.606
• Mol file: 287180-12-5.mol

Synonyms:

Chemical Property of (2-chlorobenzyl)ferrocene

Chemical Property:

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Technology Process of (2-chlorobenzyl)ferrocene

There total 1 articles about (2-chlorobenzyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

o‐chlorobenzoylferrocene (49547-67-3) + borane tetrahydrofuran → (2-chlorobenzyl)ferrocene (287180-12-5)

Guidance literature:

In tetrahydrofuran; BH3*THF (1.1 equiv. of a 0.8 M solution in THF) added at room temp. to asoln. of the ferrocenyl ketone (1.0 equiv.) in THF, stirred at room tem p. overnight, water added; extracted with chloroform, dried (MgSO4), concentrated in vacuo, crude product purified by flash column chromatography on silica gel (TLC Rf 0.40 (hexane)), elem. anal.;

DOI:10.1039/b000833h

upstream raw materials:

o‐chlorobenzoylferrocene

Refernces