tetrahydrofuran-2-ylmethyl 4-nitrobenzoate

Base Information

• Chemical Name: tetrahydrofuran-2-ylmethyl 4-nitrobenzoate
• CAS No.: 4696-98-4
• Molecular Formula: C₁₂H₁₃NO₅
• Molecular Weight: 251.239
• Mol file: 4696-98-4.mol

Synonyms:Furfurylalcohol, tetrahydro-, p-nitrobenzoate (7CI,8CI); NSC 406935

Chemical Property of tetrahydrofuran-2-ylmethyl 4-nitrobenzoate

Chemical Property:

• Vapor Pressure: 7.89E-07mmHg at 25°C
• Boiling Point: 406.8°C at 760 mmHg
• Flash Point: 185.4°C
• Density: 1.288g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tetrahydrofuran-2-ylmethyl 4-nitrobenzoate

There total 2 articles about tetrahydrofuran-2-ylmethyl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tetrahydrofurfuryl alcohol (97-99-4) + 4-nitro-benzoyl chloride (122-04-3) → (+/-)-4-nitro-benzoic acid tetrahydrofurfuryl ester (4696-98-4)

Guidance literature:

With pyridine;

DOI:10.1021/ja01869a501

Reference yield:

→ (+/-)-4-nitro-benzoic acid tetrahydrofurfuryl ester (4696-98-4)

Guidance literature:

Beim Erhitzen einer Lsg. von Tetrahydrofurfurylalkohol u. 4-Nitro-benzoesaeure in Toluol mit geringen Mengen Toluol-4-sulfonsaeure;

DOI:10.1039/jr9650007162

upstream raw materials:

Tetrahydrofurfuryl alcohol

4-nitro-benzoyl chloride