tetraphenylpropionatoantimony(V)

Base Information

• Chemical Name: tetraphenylpropionatoantimony(V)
• CAS No.: 127794-79-0
• Molecular Formula: C₂₇H₂₅O₂Sb
• Molecular Weight: 503.244
• Mol file: 127794-79-0.mol

Synonyms:

Chemical Property of tetraphenylpropionatoantimony(V)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraphenylpropionatoantimony(V)

There total 2 articles about tetraphenylpropionatoantimony(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

tetraphenylstibonium hydroxide (13371-35-2,19638-16-5) + propionic acid (802294-64-0,79-09-4) → tetraphenylpropionatoantimony(V) (127794-79-0,177481-67-3)

Guidance literature:

In propionic acid; Ph4SbOH was dissolved in propionic acid with heating at 60°C; soln. was concd. under reduced pressure, toluene was added, solvent was evapd.;

DOI:10.1023/A:1024883328867

Reference yield: 90.0%

pentaphenylantimony (2170-05-0) + propionic acid (802294-64-0,79-09-4) → tetraphenylpropionatoantimony(V) (127794-79-0,177481-67-3)

Guidance literature:

In toluene; byproducts: benzene; room temp., 1 h; evapn., washing (hexane), drying (vac.); elem. anal.;

DOI:10.1007/BF01433760

Reference yield: 99.0%

tetraphenylpropionatoantimony(V) (127794-79-0,177481-67-3) → tetraphenylantimony(V) chloride (19638-17-6,16894-68-1) + propionic acid (802294-64-0,79-09-4)

Guidance literature:

With aq. HCl;

DOI:10.1007/BF01433760

upstream raw materials:

pentaphenylantimony

propionic acid

tetraphenylstibonium hydroxide

Downstream raw materials:

triphenylantimony

methyl cinnamate

tetraphenylantimony(V) chloride

propionic acid

Refernces

• 1、 Sharutina,Sharutin,Senchurin,Fukin,Zakharov,Yanovsky,Struchkov. "Synthesis and thermal decomposition of derivatives of acyloxytetraphenylantimony". . p. 186 - 190. Retrieved 2007/10/03.