acetic acid-(2,6-dibenzyl-phenyl ester)

Base Information

• Chemical Name: acetic acid-(2,6-dibenzyl-phenyl ester)
• CAS No.: 102599-31-5
• Molecular Formula: C₂₂H₂₀O₂
• Molecular Weight: 316.4
• Mol file: 102599-31-5.mol

Synonyms:

Chemical Property of acetic acid-(2,6-dibenzyl-phenyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid-(2,6-dibenzyl-phenyl ester)

There total 5 articles about acetic acid-(2,6-dibenzyl-phenyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + 2,6-bis(phenylmethylene)cyclohexanone (897-78-9) → acetic acid-(2,6-dibenzyl-phenyl ester) (102599-31-5)

Guidance literature:

With hydrogen bromide; acetic acid; at 52 - 55 ℃;

DOI:10.1007/BF01522080

Reference yield:

benzaldehyde (100-52-7) → acetic acid-(2,6-dibenzyl-phenyl ester) (102599-31-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / Einleiten von HCl

2: HBr; glacial acetic acid / 52 - 55 °C

With ethanol; hydrogen bromide; acetic acid;

DOI:10.1007/BF01522080

Reference yield:

2,6-bis(phenylmethylene)cyclohexanone (897-78-9) → acetic acid-(2,6-dibenzyl-phenyl ester) (102599-31-5)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium/charcoal / 200 - 250 °C / Hydrogenation_.Erhitzen des Reaktionsgemisches auf 325-330grad

2: pyridine

With pyridine; palladium on activated charcoal;

DOI:10.1039/jr9370000053

upstream raw materials:

2,6-dibenzylphenol

acetic anhydride

2,6-bis(phenylmethylene)cyclohexanone

hydrogen bromide