bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine

Base Information

• Chemical Name: bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine
• CAS No.: 83720-45-0
• Molecular Formula: C₁₅H₂₂BN
• Molecular Weight: 227.157
• Mol file: 83720-45-0.mol

Synonyms:

Chemical Property of bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine

There total 1 articles about bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

dimethylacetylene (503-17-3) + chloroborane (10388-28-0) + N-methylaniline (100-61-8) → bis(cis-2-buten-2-yl)-N-methyl-N-phenyllboranamine (83720-45-0)

Guidance literature:

In diethyl ether; acetylene added under N2 to Et2O, soln. immersed in ice bath, BH2Cl in Et2O added for 0.5 h, mixture stirred at 0°C for 1 h, then at room temp. for 1 h, soln. cooled to 0°C, aniline added, Et3N in Et2Oadded, stirred at room temp. for 4 h; filtration under N2, evapn. in vac., distn. in vac.; elem. anal.;

DOI:10.1021/ja00390a024

upstream raw materials:

dimethylacetylene

chloroborane

N-methylaniline

Refernces