(mesityl)2B(C₆F₅)

Base Information

• Chemical Name: (mesityl)2B(C₆F₅)
• CAS No.: 883733-78-6
• Molecular Formula: C₂₄H₂₂BF₅
• Molecular Weight: 416.242
• Mol file: 883733-78-6.mol

Synonyms:

Chemical Property of (mesityl)2B(C₆F₅)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (mesityl)2B(C₆F₅)

There total 9 articles about (mesityl)2B(C₆F₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

(pentafluorophenyl)copper (18206-43-4) + dimesitylbromoborane (612844-47-0) → (mesityl)2B(C6F5) (883733-78-6)

Guidance literature:

In toluene; byproducts: CuBr; under Ar/N2; by cooling a soln. of Cu-contg. compd. (2.60 mmol) in toluene to -37°C and addn. it to a soln. of Mes2BBr (2.45 mmol) in toluene at the same temp.; heating to 85°C; the mixt. was kept at this temp. for 16 h; after cooling to room temp., the insol. ppt. was removed by filtration, and volatiles were removed under vac.; sublimation at 75°C under high vac.; elem. anal.;

DOI:10.1021/om050003q

Reference yield:

[mesitylcopper]5*toluene → (mesityl)2B(C6F5) (883733-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: not given

2: toluene

In toluene;

DOI:10.1021/om050003q

Reference yield:

LiP(mesityl)2B(mesityl) → (mesityl)2B(C6F5) (883733-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: d₇-N,N-dimethylformamide

In diethyl ether; d₇-N,N-dimethylformamide;

DOI:10.1021/om050003q

upstream raw materials:

dimesitylfluoroborane

(pentafluorophenyl)trimethyltin

(pentafluorophenyl)copper

dimesitylbromoborane

Refernces