N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid

Base Information

• Chemical Name: N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid
• CAS No.: 180625-54-1
• Molecular Formula: C₁₆H₁₄N₂O₂S₂
• Molecular Weight: 330.431
• Mol file: 180625-54-1.mol

Synonyms:

Chemical Property of N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid

There total 2 articles about N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-methylquinoline-2(1H)-thione (4800-27-5) + chloramine-B (127-52-6) → N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid (180625-54-1)

Guidance literature:

In ethanol; chloroform; at 0 ℃; for 2h;

DOI:10.1080/10426509608029652

Reference yield:

1-methyl-2-quinolin-2(1H)-one (606-43-9) → N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid (180625-54-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / P₄S₁₀

2: 72 percent / ethanol; CHCl₃ / 2 h / 0 °C

With tetraphosphorus decasulfide; In ethanol; chloroform;

DOI:10.1080/10426509608029652

Reference yield: 78.0%

N-phenylsulfonyl-S-(1-methyl-1,2-dihydro-2-chinolyliden)sulfimid (180625-54-1) → N-[1-Methyl-1H-quinolin-(2E)-ylidene]-benzenesulfonamide

Guidance literature:

at 150 ℃; for 0.166667h;

DOI:10.1080/10426509608029652

upstream raw materials:

1-methylquinoline-2(1H)-thione

chloramine-B

1-methyl-2-quinolin-2(1H)-one

Refernces