bis(pentafluorophenyl)dibutylgermane

Base Information

• Chemical Name: bis(pentafluorophenyl)dibutylgermane
• CAS No.: 160422-92-4
• Molecular Formula: C₂₀H₁₈F₁₀Ge
• Molecular Weight: 520.937
• Mol file: 160422-92-4.mol

Synonyms:

Chemical Property of bis(pentafluorophenyl)dibutylgermane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of bis(pentafluorophenyl)dibutylgermane

There total 2 articles about bis(pentafluorophenyl)dibutylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

bromopentafluorobenzene (344-04-7) + dibutylgermanium dibromide (3124-22-9) → bis(pentafluorophenyl)dibutylgermane (160422-92-4)

Guidance literature:

With hexaethylphosphoric triamide; In pentane; molar ratio aryl bromide/Bu2GeBr2/P(NEt2)3 120:24:120, room temp.; removal of solvent; addn. of aq. HCl; filtration; extn. of solid (pentane); removal of solvent (evapn.); addn. of water and pyridine; stirring (50-60°C, 3 h); cooling; extn. (CH2Cl2); removal of solvent; distn.; elem. anal.;

Reference yield: 19.0%

bromopentafluorobenzene (344-04-7) + dibutylgermanium dibromide (3124-22-9) → (bromodibutylgermyl)pentafluorobenzene (171857-79-7) + bis(pentafluorophenyl)dibutylgermane (160422-92-4)

Guidance literature:

With hexaethylphosphoric triamide; In pentane; molar ratio aryl bromide/Bu2GeBr2/P(NEt2)3 120:24:120, room temp.;

upstream raw materials:

bromopentafluorobenzene

dibutylgermanium dibromide