Technology Process of cis-(4-aziridin-1-yl-phenyl)-(4-nitro-phenyl)diazene
There total 5 articles about cis-(4-aziridin-1-yl-phenyl)-(4-nitro-phenyl)diazene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / water / 3 h / 20 °C
1.2: 1 h / 0 °C
1.3: 1.33 h / 0 - 10 °C
2.1: pyridine; carbon monoxide; dmap / ethylene glycol; ethanol / 6 h / -20 °C
3.1: hydrogenchloride / diethyl ether; benzene
4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 3 h / 0 °C
5.1: (2)H8-toluene / 4 h / 10 °C / Irradiation
With
pyridine; hydrogenchloride; dmap; carbon monoxide; sodium hydride;
In
diethyl ether; ethanol; (2)H8-toluene; water; ethylene glycol; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1039/c3cc43036g
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / water / 3 h / 20 °C
1.2: 1 h / 0 °C
1.3: 1.33 h / 0 - 10 °C
2.1: pyridine; carbon monoxide; dmap / ethylene glycol; ethanol / 6 h / -20 °C
3.1: hydrogenchloride / diethyl ether; benzene
4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 3 h / 0 °C
5.1: (2)H8-toluene / 4 h / 10 °C / Irradiation
With
pyridine; hydrogenchloride; dmap; carbon monoxide; sodium hydride;
In
diethyl ether; ethanol; (2)H8-toluene; water; ethylene glycol; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1039/c3cc43036g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / diethyl ether; benzene
2: sodium hydride / mineral oil; N,N-dimethyl-formamide / 3 h / 0 °C
3: (2)H8-toluene / 4 h / 10 °C / Irradiation
With
hydrogenchloride; sodium hydride;
In
diethyl ether; (2)H8-toluene; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1039/c3cc43036g