C₂₄H₁₅BrO

Base Information

• Chemical Name: C₂₄H₁₅BrO
• CAS No.: 2088537-45-3
• Molecular Formula: C₂₄H₁₅BrO
• Molecular Weight: 399.286
• Mol file: 2088537-45-3.mol

Synonyms:

Chemical Property of C₂₄H₁₅BrO

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₅BrO

There total 4 articles about C₂₄H₁₅BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

→ C24H15BrO (2088537-45-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 80 ℃;

Reference yield: 75.0%

1-Bromo-3-iodobenzene (591-18-4) + C24H23BO3 → C24H15BrO (2088537-45-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 100 ℃; Inert atmosphere;

Reference yield:

4-phenyldibenzo[b,d]furan (74104-10-2) → C24H15BrO (2088537-45-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -10 °C

1.2: 17 h

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / toluene / 5 h / 100 °C

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 100 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium acetate; potassium carbonate; In tetrahydrofuran; ethanol; water; toluene;

upstream raw materials:

4-phenyldibenzo[b,d]furan

C₁₈H₁₁IO

1-Bromo-3-iodobenzene

Refernces

• 1、 -. "Organic electroluminescent compound, organic electroluminescent device and application thereof". . . Retrieved 2020/10/30.
• 2、 -. "Anthraquinone organic electroluminescent material and application thereof". Paragraph 0082-0085; 0090-0091; 0098-0099. . Retrieved 2019/11/14.