4,4'-oxybiphenol dihexanoate

Base Information

• Chemical Name: 4,4'-oxybiphenol dihexanoate
• CAS No.: 880134-90-7
• Molecular Formula: C₂₄H₃₀O₅
• Molecular Weight: 398.499
• Mol file: 880134-90-7.mol

Synonyms:

Chemical Property of 4,4'-oxybiphenol dihexanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-oxybiphenol dihexanoate

There total 1 articles about 4,4'-oxybiphenol dihexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-dihydroxydiphenyl ether (1965-09-9) + Hexanoyl chloride (142-61-0) → 4,4'-oxybiphenol dihexanoate (880134-90-7)

Guidance literature:

In chloroform; for 1h; Heating;

DOI:10.1080/00397910500408225

Reference yield:

4,4'-oxybiphenol dihexanoate (880134-90-7) → 2,2'-dihexanoyl-4,4'-oxybiphenol (880134-93-0)

Guidance literature:

With aluminium trichloride; at 150 ℃; for 0.5h;

DOI:10.1080/00397910500408225

Reference yield:

4,4'-oxybiphenol dihexanoate (880134-90-7) → 2,2'-dihexyl-4,4'-oxybiphenol

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / 0.5 h / 150 °C

2: AlCl₃; NaBH₄ / tetrahydrofuran / 3 h / Heating

With sodium tetrahydroborate; aluminium trichloride; In tetrahydrofuran; 1: Fries rearrangement;

DOI:10.1080/00397910500408225

upstream raw materials:

4,4'-dihydroxydiphenyl ether

Hexanoyl chloride

Downstream raw materials:

2,2'-dihexanoyl-4,4'-oxybiphenol

Refernces