p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid

Base Information

• Chemical Name: p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid
• CAS No.: 1335297-15-8
• Molecular Formula: C₂₂H₂₇N₃O₁₅
• Molecular Weight: 573.467
• Mol file: 1335297-15-8.mol

Synonyms:

Chemical Property of p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid

There total 2 articles about p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

p-nitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranosiduronic acid (1335297-05-6) → p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid (1335297-15-8)

Guidance literature:

With β-N-acetylhexosaminidase from Talaromyces flavus CCF 2686; In water; at 35 ℃; for 3.5h; pH=5; aq. sodium citrate/phosphate buffer; Enzymatic reaction;

DOI:10.1002/adsc.201100371

Reference yield:

4-nitrophenyl N-acetyl-β-D-glucosaminide (3459-18-5,50645-66-4) → p-nitrophenyl 2-acetamido-2-deoxy-β-D-gluco-pyranosyluronic acid-(1->4)-2-acetamido-2-deoxy-β-D-gluco-pyranosiduronic acid (1335297-15-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; Trametes pubescens laccase / water / 120 h / 20 °C / pH 4.5 / aq. sodium acetate buffer; Enzymatic reaction

2: β-N-acetylhexosaminidase from Talaromyces flavus CCF 2686 / water / 3.5 h / 35 °C / pH 5 / aq. sodium citrate/phosphate buffer; Enzymatic reaction

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; β-N-acetylhexosaminidase from Talaromyces flavus CCF 2686; Trametes pubescens laccase; In water;

DOI:10.1002/adsc.201100371

upstream raw materials:

p-nitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranosiduronic acid

4-nitrophenyl N-acetyl-β-D-glucosaminide

Refernces