C₂₃H₃₁Cl₂N₂O₃PSe

Base Information

• Chemical Name: C₂₃H₃₁Cl₂N₂O₃PSe
• CAS No.: 87763-40-4
• Molecular Formula: C₂₃H₃₁Cl₂N₂O₃PSe
• Molecular Weight: 564.351
• Mol file: 87763-40-4.mol

Synonyms:

Chemical Property of C₂₃H₃₁Cl₂N₂O₃PSe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₁Cl₂N₂O₃PSe

There total 3 articles about C₂₃H₃₁Cl₂N₂O₃PSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Se-(dineopentylphosphoryl)-N,N'-di-(p-chlorophenyl)isoselenourea (87763-52-8) → C23H31Cl2N2O3PSe (87763-40-4)

Guidance literature:

In diethyl ether; at 0 - 20 ℃; for 1.5h; Mechanism;

DOI:10.1021/jo00179a028

Reference yield:

Dineopentyl H-phosphonate (22289-00-5) → C23H31Cl2N2O3PSe (87763-40-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / triethylamin, selenium / benzene / 72 h / Ambient temperature

2: diethyl ether / Ambient temperature

With selenium; triethylamine; In diethyl ether; benzene;

DOI:10.1021/jo00179a028

Reference yield:

bis-(4-chloro-phenyl)-carbodiimide (838-98-2) + di-O-neopentyl hydrogen phosphoroselenoate (64643-67-0) → C23H31Cl2N2O3PSe (87763-40-4)

Guidance literature:

In diethyl ether; Ambient temperature;

DOI:10.1021/jo00179a028

upstream raw materials:

bis-(4-chloro-phenyl)-carbodiimide

di-O-neopentyl hydrogen phosphoroselenoate

Se-(dineopentylphosphoryl)-N,N'-di-(p-chlorophenyl)isoselenourea

Dineopentyl H-phosphonate

Refernces