tetraphenylphosphonium amminetribromoplatinate(II)

Base Information

• Chemical Name: tetraphenylphosphonium amminetribromoplatinate(II)
• CAS No.: 110790-63-1
• Molecular Formula: Br₃H₃NPt*C₂₄H₂₀P
• Molecular Weight: 791.219
• Mol file: 110790-63-1.mol

Synonyms:

Chemical Property of tetraphenylphosphonium amminetribromoplatinate(II)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of tetraphenylphosphonium amminetribromoplatinate(II)

There total 1 articles about tetraphenylphosphonium amminetribromoplatinate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

cis-diamminedibromoplatinum(II) (13601-52-0,14591-91-4,15978-91-3) + tetraethylammonium bromide (71-91-0) + tetraphenyl phosphonium chloride (2001-45-8) → tetraphenylphosphonium amminetribromoplatinate(II) (110790-63-1)

Guidance literature:

In N,N-dimethyl acetamide; soln. of Pt compd. and NEt4Br in Me2NCOMe is heated to 100(+-2)°C (6 h, N2-stream), cooled to room temp., MeCOOEt/C6H14 is added, mixt. is chilled (12 h at -10°C), oil is dissolved in H2O, filtn., Ph4PCl in H2O is added, stirred for 30 min; solid is collected, washed with water, dried in vac.; elem. anal.;

DOI:10.1016/S0020-1693(00)87896-2

upstream raw materials:

cis-diamminedibromoplatinum(II)

tetraethylammonium bromide

tetraphenyl phosphonium chloride