Technology Process of C25H33N5O3S2
There total 4 articles about C25H33N5O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-(2-(dimethylamino)ethyl)piperazine; carbon disulfide;
With
sodium hydroxide;
In
ethanol;
at 20 ℃;
for 1h;
Cooling with ice;
2-Chloro-1-[3-furan-2-yl-5-(4-methoxy-phenyl)-4,5-dihydro-pyrazol-1-yl]-ethanone;
In
acetone;
at 20 ℃;
for 3h;
DOI:10.1002/ardp.201200384
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / acetone / 2 h / 20 °C / Cooling with ice
2.1: sodium hydroxide / ethanol / 1 h / 20 °C / Cooling with ice
2.2: 3 h / 20 °C
With
triethylamine; sodium hydroxide;
In
ethanol; acetone;
DOI:10.1002/ardp.201200384
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / ethanol; water / 5 h / 20 °C
2.1: hydrazine hydrate / ethanol / 3 h / Reflux
3.1: triethylamine / acetone / 2 h / 20 °C / Cooling with ice
4.1: sodium hydroxide / ethanol / 1 h / 20 °C / Cooling with ice
4.2: 3 h / 20 °C
With
hydrazine hydrate; triethylamine; sodium hydroxide;
In
ethanol; water; acetone;
1.1: |Claisen-Schmidt Condensation;
DOI:10.1002/ardp.201200384