trans,trans-2,8-Decadiene

Base Information

• Chemical Name: trans,trans-2,8-Decadiene
• CAS No.: 19398-85-7
• Molecular Formula: C10H18
• Molecular Weight: 138.253
• Nikkaji Number: J798.331J
• Mol file: 19398-85-7.mol

Synonyms:trans,trans-2,8-Decadiene;(2E,8E)-deca-2,8-diene;2,8-Decadiene;64460-98-6;(2E,8E)-2,8-Decadiene;19398-85-7;2,8-Decadiene, (E,E);ZIWONNNFUQQNAZ-GGWOSOGESA-N;AKOS006271805

Chemical Property of trans,trans-2,8-Decadiene

Chemical Property:

• Vapor Pressure: 2.39mmHg at 25°C
• Boiling Point: 166°Cat760mmHg
• Flash Point: 43.4°C
• PSA: 0.00000
• Density: 0.764g/cm³
• LogP: 3.69900
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 138.140850574
• Heavy Atom Count: 10
• Complexity: 84.6

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC=CCCCCC=CC
• Isomeric SMILES: C/C=C/CCCC/C=C/C

Technology Process of trans,trans-2,8-Decadiene

There total 2 articles about trans,trans-2,8-Decadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-undecenoic acid (112-38-9) → 1,10-decadiene (1647-16-1) + trans,trans-2,8-decadiene (19398-85-7) + dipropyl-1,3-butadiene (55682-65-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.17 h / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: palladium dichloride; lithium chloride / 16 h / 155 - 160 °C / Inert atmosphere; Schlenk technique; Sealed tube

With triethylamine; lithium chloride; palladium dichloride; In dichloromethane;

DOI:10.1039/c4cc09003a

Reference yield:

4-nitrophenyl ω-undecenoate (151309-96-5) → 1,10-decadiene (1647-16-1) + trans,trans-2,8-decadiene (19398-85-7) + dipropyl-1,3-butadiene (55682-65-0)

Guidance literature:

With lithium chloride; palladium dichloride; at 155 - 160 ℃; for 16h; Overall yield = 32 %; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1039/c4cc09003a

upstream raw materials:

10-undecenoic acid

4-nitrophenyl ω-undecenoate

Refernces