1RS, 2RS-1-acetoxy-1,2,3-trichloropropane

Base Information

• Chemical Name: 1RS, 2RS-1-acetoxy-1,2,3-trichloropropane
• CAS No.: 55704-82-0
• Molecular Formula: C₅H₇Cl₃O₂
• Molecular Weight: 205.468
• Mol file: 55704-82-0.mol

Synonyms:

Chemical Property of 1RS, 2RS-1-acetoxy-1,2,3-trichloropropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1RS, 2RS-1-acetoxy-1,2,3-trichloropropane

There total 4 articles about 1RS, 2RS-1-acetoxy-1,2,3-trichloropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-1,3-Dichloropropene (10061-01-5) → 2-acetoxy-1,1,3-trichloropropane (55704-81-9) + 2-fluoro-1,1,3-trichloropropane (76937-36-5) + threo-1-Fluor-1,2,3-trichlorpropan (67832-44-4,67832-50-2,76985-33-6,76985-34-7,84847-79-0,84847-80-3) + 1RS, 2RS-1-acetoxy-1,2,3-trichloropropane (55704-82-0,67832-47-7,84815-99-6,84816-12-6)

Guidance literature:

With chlorine monofluoride; In 1,1,2-Trichloro-1,2,2-trifluoroethane; ethyl acetate; at 20 - 25 ℃; for 30h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

(E)-1,3-dichloro-prop-1-ene (10061-02-6) → 2-acetoxy-1,1,3-trichloropropane (55704-81-9) + 2-fluoro-1,1,3-trichloropropane (76937-36-5) + 1RS, 2SR-1-fluoro-1,2,3-trichloropropane (67832-44-4,67832-50-2,76985-33-6,76985-34-7,84847-79-0,84847-80-3) + 1RS, 2SR-1-acetoxy-1,2,3-trichloropropane (55704-82-0,67832-47-7,84815-99-6,84816-12-6)

Guidance literature:

With chlorine monofluoride; In 1,1,2-Trichloro-1,2,2-trifluoroethane; ethyl acetate; at 20 - 25 ℃; for 30h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

ethyl acetate (141-78-6) + (E)-1,3-dichloro-prop-1-ene (10061-02-6) → 2-acetoxy-1,1,3-trichloropropane (55704-81-9) + 2-fluoro-1,1,3-trichloropropane (76937-36-5) + 1RS, 2SR-1-fluoro-1,2,3-trichloropropane (67832-44-4,67832-50-2,76985-33-6,76985-34-7,84847-79-0,84847-80-3) + 1RS, 2SR-1-acetoxy-1,2,3-trichloropropane (55704-82-0,67832-47-7,84815-99-6,84816-12-6)

Guidance literature:

With chlorine monofluoride; In 1,1,2-Trichloro-1,2,2-trifluoroethane; at 20 - 25 ℃; for 30h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

upstream raw materials:

(E)-1,3-dichloro-prop-1-ene

ethyl acetate

cis-1,3-Dichloropropene

Refernces