1,3-Disilaindane

Base Information

• Chemical Name: 1,3-Disilaindane
• CAS No.: 4361-65-3
• Molecular Formula: C₇H₁₀Si₂
• Molecular Weight: 150.327
• Mol file: 4361-65-3.mol

Synonyms:1,3-Disilaindan(7CI,8CI)

Chemical Property of 1,3-Disilaindane

Chemical Property:

• Boiling Point: 75 - 76 °C (10 mmHg)
• PSA: 0.00000
• LogP: -1.33580

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Disilaindane

There total 3 articles about 1,3-Disilaindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,3,3-tetrachloro-2,3-dihydro-1H-benzo[1,3]disilole (16538-74-2) → 1,3-Disilaindan (4361-65-3)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Heating;

Reference yield:

dichloromethylphenylsilane (149-74-6) → 1,3-Disilaindan (4361-65-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Si₂Cl₆, SiCl₄ / 680 °C

2: LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; tetrachlorosilane; hexachlorodisilane; In diethyl ether;

Reference yield:

→ 1,3-Disilaindan (4361-65-3)

Guidance literature:

Neben anderen Verbb. bei der Pyrolyse von CH3-SiCl3, (CH3)2SiCl2 od. (CH3)3SiCl u. Hydrieren des Rkgem. mit LiAlH4 in Ae. oder THF unter N2;

DOI:10.1002/zaac.19643270311

upstream raw materials:

1,1,3,3-tetrachloro-2,3-dihydro-1H-benzo[1,3]disilole

dichloromethylphenylsilane