benzoic acid benzo[h]quinolin-3-yl ester

Base Information

• Chemical Name: benzoic acid benzo[h]quinolin-3-yl ester
• CAS No.: 102159-96-6
• Molecular Formula: C₂₀H₁₃NO₂
• Molecular Weight: 299.329
• Mol file: 102159-96-6.mol

Synonyms:

Chemical Property of benzoic acid benzo[h]quinolin-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzoic acid benzo[h]quinolin-3-yl ester

There total 3 articles about benzoic acid benzo[h]quinolin-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,4-tetrahydrobenzo[h]quinoline (5223-80-3) → benzoic acid benzo[h]quinolin-3-yl ester (102159-96-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; phenol / 210 °C

2: pyridine

With pyridine; nickel; phenol;

Reference yield:

benzo[h]quinolin-3-ol (91804-13-6) + benzoyl chloride (98-88-4) → benzoic acid benzo[h]quinolin-3-yl ester (102159-96-6)

Guidance literature:

With pyridine;

Reference yield:

3-hydroxy-7,8-benzo-1,2,3,4-tetrahydroquinoline (5423-67-6) → benzoic acid benzo[h]quinolin-3-yl ester (102159-96-6)

Guidance literature:

Multi-step reaction with 2 steps

1: cyclohexanone; aluminium phenolate; toluene / 125 °C

2: pyridine

With pyridine; aluminium(III) phenoxide; cyclohexanone; toluene;

upstream raw materials:

benzo[h]quinolin-3-ol

benzoyl chloride

3-hydroxy-7,8-benzo-1,2,3,4-tetrahydroquinoline

1,2,3,4-tetrahydrobenzo[h]quinoline