6-(3,4-Dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(Z)-(2,4,6-trimethylphenyl)imino]-2(1H)-pyrimidinone

Base Information

• Chemical Name: 6-(3,4-Dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(Z)-(2,4,6-trimethylphenyl)imino]-2(1H)-pyrimidinone
• CAS No.: 117321-77-4
• Molecular Formula: C24H29 N3 O3
• Molecular Weight: 407.51
• Mol file: 117321-77-4.mol

Synonyms:2(1H)-Pyrimidinone,6-(3,4-dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(2,4,6-trimethylphenyl)imino]-,(E)-; FR 58664

Chemical Property of 6-(3,4-Dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(Z)-(2,4,6-trimethylphenyl)imino]-2(1H)-pyrimidinone

Chemical Property:

• Boiling Point: 558.5±60.0 °C(Predicted)
• PKA: 9.59±0.20(Predicted)
• PSA: 57.75000
• Density: 1.12±0.1 g/cm3(Predicted)
• LogP: 4.04850

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-(3,4-Dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(Z)-(2,4,6-trimethylphenyl)imino]-2(1H)-pyrimidinone

There total 3 articles about 6-(3,4-Dimethoxyphenyl)-1-ethyl-3,4-dihydro-3-methyl-4-[(Z)-(2,4,6-trimethylphenyl)imino]-2(1H)-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-6-(3,4-dimethoxyphenyl)-3-methyl-4-(2,4,6-trimethylphenylimino)-2(1H)-pyrimidinone + ethyl iodide (75-03-6) → (4E)-6-(3,4-dimethoxyphenyl)-1-ethyl-4-(mesitylimino)-3-methyl-3,4-dihydro-2(1H)pyrimidinone (117321-77-4,94936-90-0)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide;

Reference yield:

3,4-dihydro-6-(3,4-dimethoxyphenyl)-1-ethyl-3-methyl-4-thioxo-2(1H)-pyrimidinone + 2,4,6-trimethylaniline (88-05-1) + methyl iodide (74-88-4) → (4E)-6-(3,4-dimethoxyphenyl)-1-ethyl-4-(mesitylimino)-3-methyl-3,4-dihydro-2(1H)pyrimidinone (117321-77-4,94936-90-0)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; hexane; chloroform; di-isopropyl ether;

Reference yield:

→ (4E)-6-(3,4-dimethoxyphenyl)-1-ethyl-4-(mesitylimino)-3-methyl-3,4-dihydro-2(1H)pyrimidinone (117321-77-4,94936-90-0)

Guidance literature:

upstream raw materials:

2,4,6-trimethylaniline

methyl iodide

ethyl iodide

Refernces