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Diazene, (3-methylphenyl)phenyl-

Base Information Edit
  • Chemical Name:Diazene, (3-methylphenyl)phenyl-
  • CAS No.:17478-66-9
  • Molecular Formula:C13H12N2
  • Molecular Weight:196.252
  • Hs Code.:
  • Mol file:17478-66-9.mol
Diazene, (3-methylphenyl)phenyl-

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Chemical Property of Diazene, (3-methylphenyl)phenyl- Edit
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Technology Process of Diazene, (3-methylphenyl)phenyl-

There total 11 articles about Diazene, (3-methylphenyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In ethanol; at 60 ℃; for 12h; Green chemistry;
DOI:10.1039/d0ob00103a
Guidance literature:
3-(trimethylstannyl)azobenzene; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.1h; Schlenk technique; Inert atmosphere;
methyl iodide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 13h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201500003

Reference yield: 82.0%

Guidance literature:
With oxygen; In chloroform-d1; at 160 ℃; for 24h; under 4500.45 Torr;
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