Benzenethiol, 4-nitro-,sodium salt (1:1)

Base Information

• Chemical Name: Benzenethiol, 4-nitro-,sodium salt (1:1)
• CAS No.: 13113-79-6
• Molecular Formula: C6H5 N O2 S . Na
• Molecular Weight: 177.159
• Mol file: 13113-79-6.mol

Synonyms:Benzenethiol,4-nitro-, sodium salt (9CI); Benzenethiol, p-nitro-, sodium deriv. (6CI);Benzenethiol, p-nitro-, sodium salt (8CI); Sodium, [(p-nitrophenyl)thio]-(7CI); 4-Nitrobenzenethiol sodium salt; 4-Nitrothiophenol sodium salt; Sodium4-nitrobenzenethiolate; Sodium 4-nitrophenyl sulfide; Sodium4-nitrothiophenolate; Sodium 4-nitrothiophenoxide; Sodium p-nitrobenzenethiolate;Sodium p-nitrophenylmercaptide; Sodium p-nitrothiophenolate; Sodiump-nitrothiophenoxide; p-Nitrothiophenol sodium salt

Chemical Property of Benzenethiol, 4-nitro-,sodium salt (1:1)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenethiol, 4-nitro-,sodium salt (1:1)

There total 9 articles about Benzenethiol, 4-nitro-,sodium salt (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzonitrile (100-00-5) → bis(4-nitrophenyl)sulfide (1223-31-0) + sodium 4-nitrobenzenethiolate (13113-79-6)

Guidance literature:

With sodium sulfide; biphenyl; In N,N-dimethyl-formamide; at 120 ℃; Product distribution; var. times;

DOI:10.1021/jo00163a013

Reference yield:

1-acetylsulfanyl-4-nitro-benzene (15119-62-7) → sodium acetate (127-09-3) + sodium 4-nitrobenzenethiolate (13113-79-6)

Guidance literature:

With sodium hydroxide; In water; acetonitrile; at 25 ℃; Kinetics;

DOI:10.1139/v05-157

Reference yield:

para-nitrobenzenethiol (1849-36-1) → sodium 4-nitrobenzenethiolate (13113-79-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

upstream raw materials:

bis(4-nitrophenyl)sulfide

4-chlorobenzonitrile

S-(4-nitrophenyl) diphenylphosphinothioate

1-acetylsulfanyl-4-nitro-benzene

Downstream raw materials:

bis(4-nitrophenyl)sulfide

3-(4-nitrophenylsulfanyl)-propanoic acid

benzaldehyde-[bis-(4-nitro-phenyl)-dithioacetal]

6-methyl-2-(4-nitro-phenylsulfanyl)-pyrimidin-4-ylamine

Refernces

• 1、 Yadav, Vishal,Siegler, Maxime A.,Goldberg, David P.. "Temperature-Dependent Reactivity of a Non-heme FeIII(OH)(SR) Complex: Relevance to Isopenicillin N Synthase". . p. 46 - 52. Retrieved 2021.
• 2、 Hu, Bowen,Chen, Dafa,Hu, Xile. "Reversible dimerization of mononuclear models of [Fe]-hydrogenase". supporting information. p. 6221 - 6224. Retrieved 2013/07/05.