3-Nonanol

Base Information

• Chemical Name: 3-Nonanol
• CAS No.: 185019-15-2
• Molecular Formula: C9H20O
• Molecular Weight: 144.257
• Mol file: 185019-15-2.mol

Synonyms:

Chemical Property of 3-Nonanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Nonanol

There total 12 articles about 3-Nonanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

heptanal (111-71-7) + C4H10Zn*C2H5Li → nonan-3-ol (185019-15-2) + n-heptan1ol (111-70-6)

Guidance literature:

In toluene; for 24h; Title compound not separated from byproducts.;

DOI:10.1021/jo000630j

Reference yield: 90.0%

heptanal (111-71-7) + ethyl sodium ; compound with diethyl zinc → nonan-3-ol (185019-15-2) + tetradecane-7,8-diol (16000-65-0) + n-heptan1ol (111-70-6)

Guidance literature:

In toluene; for 0.166667h; Title compound not separated from byproducts.;

DOI:10.1021/jo000630j

Reference yield: 85.0%

heptanal (111-71-7) + ethyl potassium ; compound with diethyl zinc → nonan-3-ol (185019-15-2) + tetradecane-7,8-diol (16000-65-0) + n-heptan1ol (111-70-6)

Guidance literature:

In toluene; for 0.166667h; Title compound not separated from byproducts.;

DOI:10.1021/jo000630j

upstream raw materials:

1-hydroxy-2-bromooctane

methylmagnesium chloride

dimethyl(phenyl)silyllithium

1,2-Epoxyoctane

Downstream raw materials:

3-nonanone

(E)-3-nonene

2-nonene

nonan-3-yl acetate

Refernces

• 1、 Takada, Yuki,Caner, Joaquim,Kaliyamoorthy, Selvam,Naka, Hiroshi,Saito, Susumu. "Photocatalytic Transfer Hydrogenolysis of Allylic Alcohols on Pd/TiO2: A Shortcut to (S)-(+)-Lavandulol". supporting information. p. 18025 - 18032. Retrieved 2017/12/08.
• 2、 Von Bühler, Clemens J.,Urlacher, Vlada B.. "A novel P450-based biocatalyst for the selective production of chiral 2-alkanols". supporting information. p. 4089 - 4091. Retrieved 2014/04/03.