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Sodium dibutyldithiocarbamate

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Name

Sodium dibutyldithiocarbamate

EINECS 205-238-0
CAS No. 136-30-1 Density 1,09 g/cm3
PSA 35.33000 LogP 2.72040
Solubility Soluble in water, non-toxic, not suitable to touch with iron container. Melting Point 123 - 125oC
Formula C9H19NS2.Na Boiling Point 257.7 °C at 760 mmHg
Molecular Weight 227.37 Flash Point 109.6 °C
Transport Information N/A Appearance Pale yellow green to light brown liquid
Safety 26-36/37/39 Risk Codes 36/37/38
Molecular Structure Molecular Structure of 136-30-1 (DibutylCarbamodithioic acid sodium salt) Hazard Symbols T,C,N
Synonyms

Carbamicacid, dibutyldithio-, sodium salt (7CI,8CI);Carbamodithioic acid, dibutyl-,sodium salt (9CI);Accel TP;Butyl Namate;Dibutyl sodium dithiocarbamate;Dibutyldithiocarbamic acid sodium salt;Nocceler TP;Pennac SDB;Silverdibutyldithiocarbamate;Sodium DBDT;Sodium N,N-dibutyldithiocarbamate;Sodiumdibutyldithiocarbamate;Tepidone;Tepidone rubber accelerator;Vulcacure NB;

Article Data 17

Sodium dibutyldithiocarbamate Synthetic route

75-15-0

carbon disulfide

111-92-2

dibutylamine

136-30-1

sodium dibutyl dithiocarbamate

Conditions
ConditionsYield
With potassium hydroxide In water at 45℃; for 6h; Temperature; Cooling with ice; Autoclave; Large scale;95.4%
With sodium hydroxide In ethanol at 0℃; for 2h;90%
Stage #1: dibutylamine With sodium hydroxide In methanol; water at 0℃; for 0.333333h;
Stage #2: carbon disulfide In methanol; water at 20℃;
84%

4(CH3)4N(1+)*2Nb(4+)*2Se2(2-)*8NCS(1-)=((CH3)4N)4(Nb2(Se2)2(NCS)8)

136-30-1

sodium dibutyl dithiocarbamate

[Nb2(μ-Se2)2(n-butyldithiocarbamate)4]

Conditions
ConditionsYield
In chloroform; water Nb complex and Na salt of ligand in H2O-CHCl3 stirred; org. layer sepd.; dried over CaCl2; diluted with EtOH; evapd. in open beaker; elem. anal.;100%

4(C2H5)4N(1+)*2Nb(4+)*2S2(2-)*8NCS(1-)=((C2H5)4N)4(Nb2(S2)2(NCS)8)

136-30-1

sodium dibutyl dithiocarbamate

[Nb2(μ-S2)2(n-butyldithiocarbamate)4]

Conditions
ConditionsYield
In water Nb complex added to soln. of Na salt of ligand in water; stirred for 12 h; filtered; ppt. washed with MeOH and then quickly with small amt. of Et2O; dried in vac.; elem. anal.;100%

3-(1-benzotriazolyl)propyl-2-chloroacetate

136-30-1

sodium dibutyl dithiocarbamate

C20H30N4O2S2

Conditions
ConditionsYield
In tetrahydrofuran for 5.5h; Reflux;89.8%
136-30-1

sodium dibutyl dithiocarbamate

1634-02-2

tetrabutylthiuram Disulfide

Conditions
ConditionsYield
In water at 25℃; Electrolysis; Flow reactor;88%

C11H15ClN2O2S

136-30-1

sodium dibutyl dithiocarbamate

C20H33N3O2S3

Conditions
ConditionsYield
In tetrahydrofuran for 5.5h; Reflux;85.8%

uranyl nirate hexahydrate

136-30-1

sodium dibutyl dithiocarbamate

791-28-6

Triphenylphosphine oxide

112614-55-8

bis(N,N-di(n-butyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI)

Conditions
ConditionsYield
In methanol; dimethyl sulfoxide byproducts: sodium nitrate; a soln. of 1 equiv of UO2(NO3)2*6H2O in MeOH-DMSO was treated with 1 equiv of Ph3PO and 2 equiv of n-Bu2NCS2Na, stirred for 30 min at room. temp.; filtered, pptd. by adding H2O to the filtrate, filtered by suction, washed with H2O, dried over CaCl2 under vac., purified by dissolving in MeOH-DMSO and reprecipitating with H2O; elem. anal.;85%
150-11-8

N,N'-dibutyldithiocarbamic acid

294673-79-3, 34408-87-2

(diphenyl-tert-butylphosphine)2PdCl2

136-30-1

sodium dibutyl dithiocarbamate

[Pd(dibutyldithiocarbamate)(diphenyl-tert-butylphosphine)Cl]

Conditions
ConditionsYield
In dichloromethane for 24h; Reflux;83%
75-09-2

dichloromethane

136-30-1

sodium dibutyl dithiocarbamate

10254-57-6

methylene bis-(di-n-butylamino-dithioformate)

Conditions
ConditionsYield
With poly(ethylene glycol) 1,500 (PEG-1,500) In water for 12h; Ambient temperature;80%

bismuth (III) nitrate pentahydrate

136-30-1

sodium dibutyl dithiocarbamate

1000068-54-1, 34410-99-6

tris(di-n-butyldithiocarbamato)bismuth(III) complex

Conditions
ConditionsYield
Stage #1: bismuth (III) nitrate pentahydrate In ethanol for 1h;
Stage #2: sodium dibutyl dithiocarbamate In ethanol at 20℃; for 4h;
80%

Sodium dibutyldithiocarbamate Specification

The Sodium dibutyldithiocarbamate with the cas number 136-30-1. It is also called sodium N,N-dibutylcarbamodithioate, which is also it's IUPAC name, and it's system Names are (1) Carbamic acid, dibutyldithio-, sodium salt ; (2) Carbamodithioic acid, N,N-dibutyl-, sodium salt (1:1) ; (3) Carbamodithioic acid, dibutyl-, sodium salt. It belongs to the following product categories: Biphenyl & Diphenyl ether.

Physical properties about Sodium dibutyldithiocarbamate are: (1)ACD/LogP: 3.93 ; (2)# of Rule of 5 Violations: 0 ; (3)ACD/LogD (pH 5.5): 1.51 ; (4)ACD/LogD (pH 7.4): 0.28 ; (5)ACD/BCF (pH 5.5): 2.16 ; (6)ACD/BCF (pH 7.4): 1 ; (7)ACD/KOC (pH 5.5): 12.35 ; (8)ACD/KOC (pH 7.4): 1 ; (9)#H bond acceptors: 1 ; (10)#H bond donors: 0 ; (11)#Freely Rotating Bonds: 6 ; (12)Polar Surface Area: 74.13 Å2 ; (13)Flash Point: 109.6 °C ; (14)Enthalpy of Vaporization: 49.52 kJ/mol ; (15)Boiling Point: 257.7 °C at 760 mmHg ; (16)Vapour Pressure: 0.0144 mmHg at 25°C

Uses of Sodium dibutyldithiocarbamate: Sodium dibutyldithiocarbamate can react with dichloromethane to produce dibutyl-dithiocarbamic acid dibutylthiocarbamoylsulfanylmethyl ester according to the following chemical equation with poly(ethylene glycol) 1,500 (PEG-1,500) as reagent, at ambient temperature for 12 hour(s). Yield is 80 %.
 

When you are using this chemical, please be cautious about it as the following: It is quite irritating to eyes, respiratory system and skin. When you are using this chemical, please wear suitable gloves and eye/face protection to avoid contact with skin and eyes. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure :
(1).SMILES:[Na+].[S-]C(=S)N(CCCC)CCCC
(2).InChI:InChI=1/C9H19NS2.Na/c1-3-5-7-10(9(11)12)8-6-4-2;/h3-8H2,1-2H3,(H,11,12);/q;+1/p-1

Toxic information of Mibolerone can be showed as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 300mg/kg (300mg/kg)   National Technical Information Service. Vol. AD277-689,

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