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Cas Database |
| Name |
Triethylgallium |
EINECS | 214-232-7 |
| CAS No. | 1115-99-7 | Density | 1.058 g/cm3 |
| PSA | 0.00000 | LogP | 2.54090 |
| Solubility | N/A | Melting Point |
-82.3 °C |
| Formula | C6H15Ga | Boiling Point | 143 °C |
| Molecular Weight | 156.908 | Flash Point | -18 °C |
| Transport Information | UN 3203 | Appearance | N/A |
| Safety | 16-36/37/39-43 | Risk Codes | 14/15-17 |
| Molecular Structure |
|
Hazard Symbols | F,C |
| Synonyms |
Triethylgallane; |
Article Data | 33 |
Triethylgallium Synthetic route
- 1115-99-7
triethyl gallium
| Conditions | Yield |
|---|---|
| In neat (no solvent) metal complex decomposed at 120-143°C for 2-3 h; | 93% |
| Conditions | Yield |
|---|---|
| Stage #1: triethylaluminum With tri-n-propylamine at 20℃; Stage #2: gallium(III) trichloride at 100℃; for 2h; Neat (no solvent); | 92% |
| In hexane at 70℃; Glovebox; Inert atmosphere; |
- 1115-99-7
triethyl gallium
| Conditions | Yield |
|---|---|
| In neat (no solvent) metal complex decomposed at 120-143°C for 2-3 h; | 92% |
- 1115-99-7
triethyl gallium
| Conditions | Yield |
|---|---|
| In neat (no solvent) metal complex decomposed at 120-125°C for 2-3 h; | 90% |
A
- 1115-99-7
triethyl gallium
B
- 30914-08-0
diethylgallium chloride
| Conditions | Yield |
|---|---|
| With potassium chloride; sodium chloride at 120 - 130℃; under 225.023 Torr; Pressure; Concentration; Temperature; Inert atmosphere; | A 75.9% B n/a |
| With potassium chloride; sodium chloride at 120℃; under 225.023 Torr; Inert atmosphere; | A 75.9% B 19% |
- 1115-99-7
triethyl gallium
| Conditions | Yield |
|---|---|
| In neat (no solvent) heated slowly under 1E-2 mmHg in a trap-to-trap distillation apparatus (receiver flask at -196 °C), liberation of Et3Ga started at 80 °C, the rate was more satisfactory at 120-125 °C;; | 66% |
- 7440-55-3
gallium
- 7439-95-4
magnesium
- 75-03-6
ethyl iodide
A
- 1115-99-7
triethyl gallium
B
- 7786-30-3
magnesium chloride
| Conditions | Yield |
|---|---|
| In hexane inert condition; addn. of hexane to mixt. of Mg and Ga (vac.), addn. of hexane, dropwise addn. of EtI (boiling hexane); distillation; | A 65% B n/a |
- 7440-55-3
gallium
- 7553-56-2
iodine
- 7439-95-4
magnesium
- 75-03-6
ethyl iodide
A
- 1115-99-7
triethyl gallium
B
- 7786-30-3
magnesium chloride
| Conditions | Yield |
|---|---|
| In neat (no solvent) inert condition; addn. of I2 to mixt. of Mg and Ga, heating in vac. (150°C), chilling, addn. of EtI (50 - 70°C, 1 h), heating (90 °C, 4 h); distillation; | A 61% B n/a |
| Conditions | Yield |
|---|---|
| In neat (no solvent) inert condition; addn. of I2 to alloy Mg-Ga, heating in vac. (150 °C), chilling, addn. of EtI), heating (85°C, 4 h); distillation; | A 57% B n/a |
| Conditions | Yield |
|---|---|
| With iodine; magnesium In neat (no solvent) byproducts: MgI2; inert atm.; heating (85°C); distn.; | 57% |
Triethylgallium Specification
The IUPAC name of this chemical is Triethylgallium. With the CAS registry number 1115-99-7 and EINECS registry number 214-232-7, it is also named as Gallium, triethyl-. In addition, the molecular formula is C6H15Ga and the molecular weight is 156.91.
Physical properties about this chemical are: (1)Rotatable Bond Count: 3; (2)Exact Mass: 156.042956; (3)MonoIsotopic Mass: 156.042956; (4)Heavy Atom Count: 7; (5)Complexity: 25.7; (6)Covalently-Bonded Unit Count: 1; (7)#Freely Rotating Bonds: 3 .
Uses of Triethylgallium: it is used as chemical reagent, fine chemicals, organic synthesis reagents and pharmaceutical intermediates.And it can react with 2-(2-nitro-vinyl)-furan to get 2-but-1-enyl-furan. This reaction will need reagent hexane. The reaction time is 3 hours with ambient temperature. The yield is about 49%.
When you are using this chemical, please be cautious about it as the following:
This chemical is spontaneously flammable in air. And it reacts violently with water, liberating extremely flammable gases. When you are using it, wear suitable protective clothing, gloves and eye/face protection. You should keep away from sources of ignition - No smoking. In case of fire, use ... (indicate in the space the precise type of fire-fighting equipment. If water increases the risk add - Never use water).
You can still convert the following datas into molecular structure:
(1)SMILES: [Ga](CC)(CC)CC
(2)InChI: InChI=1/3C2H5.Ga/c3*1-2;/h3*1H2,2H3;/rC6H15Ga/c1-4-7(5-2)6-3/h4-6H2,1-3H3
(3)InChIKey: RGGPNXQUMRMPRA-KMXMPSPZAO
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