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100-88-9

Basic Information
CAS No.: 100-88-9
Name: Cyclamic acid
Article Data: 21
Molecular Structure:
Molecular Structure of 100-88-9 (Cyclamic acid)
Formula: C6H13 N O3 S
Molecular Weight: 179.24
Synonyms: Cyclohexanesulfamicacid (6CI,7CI,8CI);Sulfamic acid, cyclohexyl- (9CI);Cyclamate;Cyclamic acid;Cyclohexylamidosulfuric acid;Cyclohexylaminesulfonic acid;Cyclohexylsulfamicacid;Hexamic acid;N-Cyclohexylsulfamic acid;NSC 220327;Polycat 200;
EINECS: 202-898-1
Density: 1.32g/cm3
Melting Point: 165 - 170 C (Decomposes)
Boiling Point: °Cat760mmHg
Flash Point: °C
Solubility: Soluble SOLVENT
Appearance: white crystals
Hazard Symbols: UN NO.
Safety: Suspected human carcinogen producing bladder tumors. Poison by intravenous route. Mildly toxic by ingestion. When heated to decomposition it emits toxic fumes of SOx and NOx.
Transport Information: 25kgs
PSA: 74.78000
LogP: 2.18320
Synthetic route
108-91-8

cyclohexylamine

100-88-9

cyclohexylsulfamic acid

Conditions
ConditionsYield
With chlorosulfonic acid In chloroform for 8h; Ambient temperature;72%
With chlorosulphuric acid; chloroform
With chlorosulfonic acid
With chlorosulfonic acid In acetonitrile at 20℃; for 2h;
3173-53-3

Cyclohexyl isocyanate

100-88-9

cyclohexylsulfamic acid

Conditions
ConditionsYield
With sulfuric acid; sulfur trioxide
2211-64-5

N-cyclohexyl-hydroxylamine

100-88-9

cyclohexylsulfamic acid

Conditions
ConditionsYield
With sulfur dioxide; benzene
1122-60-7

1-nitrocyclohexane

100-88-9

cyclohexylsulfamic acid

Conditions
ConditionsYield
With sodium dithionite; water; sodium phosphate
108-91-8

cyclohexylamine

sodium chloro sulfate

sodium chloro sulfate

100-88-9

cyclohexylsulfamic acid

100-88-9

cyclohexylsulfamic acid

1620401-56-0

(R)-6-methylamino-2-methylheptene

(R)-isometheptene cyclamate

Conditions
ConditionsYield
In ethanol at -20℃; Solvent; Temperature;100%
100-88-9

cyclohexylsulfamic acid

C43H51N7O9S2

(x)C6H13NO3S*C43H51N7O9S2

Conditions
ConditionsYield
In methanol at 20℃;95.6%
100-88-9

cyclohexylsulfamic acid

5-[2-[4-(1,2-benzisothiazol-3-yl)-1-piperazinyl]ethyl]-6-chloro-1,3-dihydro-2H-indol-2-one N-cyclohexylsulfamate

Conditions
ConditionsYield
In ethanol; water at -15 - 80℃;95.2%
706779-91-1

N-(1-methylpiperidin-4-yl)-N-(4-fluorophenylmethyl)-N′-(4-(2-methylpropyloxyl)phenylmethyl)carbamide

100-88-9

cyclohexylsulfamic acid

C25H34FN3O2*H2O*C6H13NO3S

Conditions
ConditionsYield
In ethyl acetate at 20 - 42℃; for 5h;93.7%
100-88-9

cyclohexylsulfamic acid

302962-49-8

dasatanib

N-(2-chloro-6-methylphenyl)-2-[6-[4-(2-hydroxyethyl)piperazin-1-yl]-2-methylpyrimidin-4-ylamino]-1,3-thiazole-5-carboxamide monocyclamate salt

Conditions
ConditionsYield
In methanol at 70℃;93.4%
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Chemistry

Chemistry informtions about  Cyclamic acid (100-88-9) is:
IUPAC Name: (2E)-2-hydroxyimino-1-phenylpropan-1-one ; -hydroxyimino-1-phenylpropan-1-one
Synonyms: Cyclohexanesulphamic acid ; cyclohexanesulphamicacid ; Cyclohexylamidosulfuric acid ; cyclohexylamidosulfuricacid ; Cyclohexylamidosulphuric acid ; cyclohexylamidosulphuricacid ; Cyclohexylaminesulfonic acid ; cyclohexylaminesulfonicacid
MF: C6H13NO3S
MW: 179.24
EINECS: 202-898-1
Melting Point:  ~180 °C (dec.)
Density: 1.32 g/cm3
Following is the molecular structure of  Cyclamic acid (100-88-9) is:

Uses

The sodium and calcium salts of  Cyclamic acid (100-88-9) are used as artificial sweeteners under the name cyclamate.This Chemical is banned in the USA and other countries for use as a sweetener. In the UK it used to be banned, but now it is allowed.This is also sometimes considered to be a carcinogen.

Toxicity Data With Reference

Organism

Test

Type

Route

Reported Dose

(Normalized

Dose)

Effect

Source

mouse

LD50

intravenous

180mg/kg

(180mg/kg)

 

U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#01774,

mouse

LD50

oral

680mg/kg

(680mg/kg)

Behavioral: convulsions or effect on seizure threshold lungs, thorax, or respiration: respiratory stimulation gastrointestinal: changes in structure or function of salivary glands

National Technical Information Service. Vol. OTS0540890,

rat

LD50

intravenous

4gm/kg

(4000mg/kg)

 

American Journal of the Medical Sciences. Vol. 225, Pg. 551, 1953.

rat

LD50

oral

12gm/kg

(12000mg/kg)

 

American Journal of the Medical Sciences. Vol. 225, Pg. 551, 1953.

Safety Profile

Safety Statements:
S22: Do not breathe dust.
S24/25: Avoid contact with skin and eyes.
WGK Germany: 2
RTECS: GV6950000