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101-38-2

Basic Information
CAS No.: 101-38-2
Name: 2,6-Dichloroquinone-4-chloroimide
Article Data: 11
Molecular Structure:
Molecular Structure of 101-38-2 (2,6-Dichloroquinone-4-chloroimide)
Formula: C6H2Cl3NO
Molecular Weight: 210.447
Synonyms: p-Benzoquinoneimine, N,2,6-trichloro- (6CI,7CI);2,6-Dichloro-4-(chloroimino)cyclohexa-2,5-dienone;2,6-Dichloro-4-N-chloroquinonimine;2,6-Dichloro-4-chloroimino-2,5-cyclohexadien-1-one;2,6-Dichloro-p-benzoquinone-4-chlorimide;2,6-DichlorobenzoquinoneN-chloroimine;2,6-Dichlorobenzoquinone chloroimide;2,6-Dichlorobenzoquinone-4-chloroimine;2,6-Dichloroquinone chloroimide;2,6-Dichloroquinone-4-chloroimide;2,6-Dichloroquinonechloroimine;Gibbs'reagent;N,2,6-Trichloro-p-benzoquinoneimine;N,2,6-Trichloro-p-benzoquinonimine;N,2,6-Trichlorobenzoquinone imine;NSC6293;Named reagents and solutions, Gibbs';
EINECS: 202-937-2
Density: 1.61 g/cm3
Melting Point: 65-67 °C(lit.)
Boiling Point: 262.3 °C at 760 mmHg
Flash Point: 104.3 °C
Solubility: insoluble in water
Appearance: yellow crystals
Hazard Symbols: FlammableF, IrritantXi, HarmfulXn, ExplosiveE
Risk Codes: 5-11-36/37/38-20/22-2
Safety: 15-26-36/37/39-33-16-36
Transport Information: UN 3224
PSA: 29.43000
LogP: 2.40930
Synthetic route
88-06-2

2,4,6-Trichlorophenol

A

101-38-2

2,6-dichloroquinone-4-chloroimide

B

697-91-6

2,6-dichloro-1,4-benzoquinone

Conditions
ConditionsYield
With sodium hydroxide; sulfuric acid In water for 0.75h; pH=6; Product distribution; Further Variations:; Reagents; pH-values;A 35%
B 55%
88-06-2

2,4,6-Trichlorophenol

A

101-38-2

2,6-dichloroquinone-4-chloroimide

B

20244-55-7

2,4,4,6-tetrachlorocyclohexa-2,5-dien-1-one

C

697-91-6

2,6-dichloro-1,4-benzoquinone

Conditions
ConditionsYield
With NHCl2 In 1,2-dimethoxyethane; water pH=6; Product distribution;A 32%
B 48%
C 20%
618-80-4

2,6-dichloro-4-nitrophenol

101-38-2

2,6-dichloroquinone-4-chloroimide

Conditions
ConditionsYield
With hydrogenchloride; tin anschliessendes Behandeln mit wss. NaOCl bei -5grad bis -3grad;
5930-28-9

4-amino-2,6-dichlorophenol

101-38-2

2,6-dichloroquinone-4-chloroimide

Conditions
ConditionsYield
With hydrogenchloride; sodium hypochlorite at 0℃;
With sodium hydroxide; chlorine
With hydrogenchloride; sodium hypochlorite In water
7647-01-0

hydrogenchloride

5930-28-9

4-amino-2,6-dichlorophenol

calcium chloride

calcium chloride

101-38-2

2,6-dichloroquinone-4-chloroimide

hydrochloride of 2.6-dichloro-4-amino-phenol

hydrochloride of 2.6-dichloro-4-amino-phenol

101-38-2

2,6-dichloroquinone-4-chloroimide

Conditions
ConditionsYield
With hydrogenchloride; calcium chloride
5930-28-9

4-amino-2,6-dichlorophenol

sodium hypochlorite

sodium hypochlorite

101-38-2

2,6-dichloroquinone-4-chloroimide

101-38-2

2,6-dichloroquinone-4-chloroimide

106-49-0

p-toluidine

C7H9N*C6H2Cl3NO

Conditions
ConditionsYield
In ethanol at 20℃; for 0.25h;91%
101-38-2

2,6-dichloroquinone-4-chloroimide

371-41-5

4-Fluorophenol

537-14-4

dichlorophenolindophenol

Conditions
ConditionsYield
With borate buffer In ethanol for 2h;78%
101-38-2

2,6-dichloroquinone-4-chloroimide

83891-03-6

norfluoxetine

C6H2Cl3NO*C16H16F3NO

Conditions
ConditionsYield
at 20℃; for 1h;71%
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  • 101-38-2 2,6-Dichloroquinone-4-chloroimide C6H2Cl3NO

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  • 2,6-Dichloroquinone-4-chloroimide cas  101-38-2

  • Casno:

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  • 2,6-DICHLOROQUINONE-4-CHLORIMIDE

  • Casno:

    101-38-2

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  • 101-38-2             C6H2Cl3NO             2,6-Dichloroquinone-4-chloroimide

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Chemistry

IUPAC Name: 2,6-Dichloroquinone-4-chloroimide
The MF of 2,6-Dichloroquinone-4-chloroimide (101-38-2) is C6H2Cl3NO.

                                      
The MW of 2,6-Dichloroquinone-4-chloroimide (101-38-2) is 210.45.
Synonyms of 2,6-Dichloroquinone-4-chloroimide (101-38-2): 2,6-Dichloro-4-benzoquinone 4-chlorimine ; 2,5-Cyclohexadien-1-one, 2,6-dichloro-4-(chloroimino)- ; 2,6-Dichloro-4-(chloroimino)-2,5-cyclohexadien-1-one ; N,2,6-Trichloro-p-quinoneimine Product Categories: Anthraquinones, Hydroquinones and Quinones
Index of Refraction: 1.612
Form: yellow crystals  
EINECS: 202-937-2
Density: 1.61 g/ml 
Flash Point: 104.3 °C
Boiling Point: 262.3 °C
Melting Point: 67 °C
Water Solubility: Insoluble
Stability: Stable
Merck: 4421

Toxicity Data With Reference

1.    

ipr-mus LD50:20 mg/kg

    JMCMAR    Journal of Medicinal Chemistry. 21 (1978),11.
2.    

ivn-mus LD50:56 mg/kg

    CSLNX*    U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#00254 .

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal and intravenous routes. A storage hazard. It may explode at room temperature. When heated to decomposition it emits very toxic fumes of Cl and NOx.
Safety information of 2,6-Dichloroquinone-4-chloroimide (101-38-2):
Hazard Codes  F,Xi,Xn,E
Risk Statements 
5  Heating may cause an explosion
11  Highly Flammable
36/37/38  Irritating to eyes, respiratory system and skin
20/22  Harmful by inhalation and if swallowed
Safety Statements 
15  Keep away from heat
26  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36/37/39  Wear suitable protective clothing, gloves and eye/face protection
33  Take precautionary measures against static discharges
16  Keep away from sources of ignition - No smoking
36  Wear suitable protective clothing
RIDADR  UN 3224 4.1
WGK Germany  3
RTECS  GU5470000
F  21