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102266-15-9

Basic Information
CAS No.: 102266-15-9
Name: 2-Amino-3-nitro-6-phenylpyridine
Article Data: 8
Molecular Structure:
Molecular Structure of 102266-15-9 (2-Amino-3-nitro-6-phenylpyridine)
Formula: C11H9N3O2
Molecular Weight: 215.211
Synonyms: 2-Pyridinamine, 3-nitro-1-phenyl- (9CI);
Density: 1.327±0.06 g/cm3(Predicted)
Melting Point: 147-149 °C(Solv: ethanol (64-17-5); water (7732-18-5))
Boiling Point: 412.6±45.0 °C(Predicted)
PSA: 84.73000
LogP: 3.34340
Synthetic route
71090-35-2

1,1-diamino-2-nitroethene

31919-75-2

3-Dimethylamino-1-phenyl-2-propen-1-on

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
With acetic acid In ethanol for 4h; Heating;80%
27048-04-0

2-amino-6-chloro-3-nitropyridine

98-80-6

phenylboronic acid

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
Stage #1: 2-amino-6-chloro-3-nitropyridine; phenylboronic acid With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate In water; toluene for 0.333333h; Inert atmosphere;
Stage #2: With tris-(dibenzylideneacetone)dipalladium(0) In water; toluene Inert atmosphere; Reflux;
75%
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; water; toluene at 90℃; for 12h;53%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 80 - 85℃; for 12h; Inert atmosphere;
31919-75-2

3-Dimethylamino-1-phenyl-2-propen-1-on

13623-94-4

1,1-di(methylsulfanyl)-2-nitroethylene

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
With ammonium acetate In ethanol for 6h; Heating;65%
13514-88-0

nitroacetamidine

sodiobenzoylacetaldehyde

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
With hydrogenchloride In ethanol for 16h; Heating;60%
84487-04-7

6-bromo-3-nitro-pyridin-2-ylamine

98-80-6

phenylboronic acid

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; ethanol; water at 100℃; for 0.5h; Inert atmosphere; Microwave irradiation;56%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; ethanol; water at 100℃; for 0.5h; Inert atmosphere; Microwave irradiation;0.280 g
1131-80-2, 1201-93-0, 31919-75-2

(E)-3-(N,N-dimethylamino)-1-phenyl-2-propen-1-one

71090-35-2

1,1-diamino-2-nitroethene

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
With acetic acid In ethanol Heating;
16013-85-7

2,6-dicholoro-3-nitropyridine

102266-15-9

2-amino-3-nitro-6-phenylpyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: ammonia / ethanol / 3 h / 0 °C
2.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate / water; toluene / 0.33 h / Inert atmosphere
2.2: Inert atmosphere; Reflux
View Scheme
102266-15-9

2-amino-3-nitro-6-phenylpyridine

144563-51-9

2,3-Diamino-6-phenylpyridin

Conditions
ConditionsYield
Stage #1: 2-amino-3-nitro-6-phenylpyridine With hydrogenchloride; iron In methanol; water at 20 - 80℃; for 1h;
Stage #2: With sodium hydroxide In methanol; water at 0℃;
99%
With hydrogen; palladium on activated charcoal In ethyl acetate under 2625.2 Torr; for 1.5h; Ambient temperature;96%
68819-84-1

tert-butyl N-(4-bromobenzyl)carbamate

102266-15-9

2-amino-3-nitro-6-phenylpyridine

C23H24N4O4

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In tetrahydrofuran for 17h; Inert atmosphere;92%
1032350-06-3

tert-butyl (1-(4-bromophenyl)cyclobutyl)carbamate

102266-15-9

2-amino-3-nitro-6-phenylpyridine

1439394-28-1

tert-butyl (1-(4-((3-nitro-6-phenylpyridin-2-yl)amino)phenyl)cyclobutyl)carbamate

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In tetrahydrofuran at 70℃; Inert atmosphere;75%
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