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Basic Information
| CAS No.: | 103-01-5 |
|---|---|
| Name: | Anilinoacetic acid |
| Article Data: | 101 |
| Molecular Structure: | |
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| Formula: | C8H9NO2 |
| Molecular Weight: | 151.165 |
| Synonyms: | H-DL-Phg-OH;TR-NPG;(Phenylamino)aceticacid;Acetic acid, (phenylamino)-;Anilinoacetic acid;N-(Phenylamino)aceticacid;N-Phenylglycine;NSC 83567; |
| EINECS: | 203-070-2 |
| Density: | 1.259 g/cm3 |
| Melting Point: | 121-127 °C |
| Boiling Point: | 359 °C at 760 mmHg |
| Flash Point: | 170.9 °C |
| Solubility: | moderately soluble in water |
| Appearance: | ochre to yellow-brown fine powder |
| Risk Codes: | 36/37/38 |
| Safety: | 22-24/25 |
| PSA: | 49.33000 |
| LogP: | 1.25610 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: ethyl bromoacetate; aniline With silica gel at 20℃; for 0.116667h; microwave irradiation; Stage #2: With sodium hydroxide In ethanol for 0.166667h; Heating; | 93% |
| Stage #1: ethyl bromoacetate; aniline With potassium carbonate for 1.5h; Milling; Stage #2: With potassium hydroxide for 1.5h; Milling; | 91% |
| Stage #1: ethyl bromoacetate; aniline Stage #2: With sodium hydroxide |
Conditions
| Conditions | Yield |
|---|---|
| 90% |
- 65171-67-7
tert-butyl 2-(phenylamino)acetate
- 103-01-5
N-Phenylglycine
Conditions
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid In dichloromethane for 3h; | 90% |
| In water; isopropyl alcohol at 200℃; for 0.25h; Solvent; Temperature; Flow reactor; | 77% |
Conditions
| Conditions | Yield |
|---|---|
| With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 75 - 80℃; for 72h; | 87% |
| With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; | 82% |
| With copper(I) oxide; caesium carbonate at 100℃; for 0.666667h; Sealed tube; Microwave irradiation; | 10% |
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; potassium carbonate In water at 90℃; for 0.833333h; Microwave irradiation; Green chemistry; | 81% |
| With pectin-stabilized copper nanoparticles In dimethyl sulfoxide at 110℃; for 2h; | 71% |
| With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 90℃; | 62% |
| With copper(l) iodide; potassium carbonate In N,N-dimethyl acetamide at 90℃; |
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In water for 0.5h; Heating; | 73% |
| With sodium hydroxide for 0.5h; Heating; | 70% |
| Stage #1: N-phenylglycine ethyl ester With sodium hydroxide In water for 0.5h; Reflux; Stage #2: With hydrogenchloride In water pH=2; |
- 178695-68-6, 181121-53-9
1-phenyl-4-oximinoimidazolidine
- 103-01-5
N-Phenylglycine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride Hydrolysis; | 60% |
- 591-50-4
iodobenzene
- 556-50-3
glycylglycine
A
- 852380-00-8
N-(N-phenyl-glycyl)-glycine
B
- 103-01-5
N-Phenylglycine
Conditions
| Conditions | Yield |
|---|---|
| With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 70℃; for 16h; | A 40% B 27% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid Electrolysis.elektrolytische Reduktion; |
Conditions
| Conditions | Yield |
|---|---|
| With potassium cyanide; ethanol |
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Anilinoacetic acid
Chemistry
The molecular formula of N-phenylglycine(103-01-5) is C8H9NO2 and its formula weight is 151.16.
N-phenylglycine(103-01-5) has a melting point of 121-123 °C(lit.).
The chemical synonyms of N-phenylglycine(103-01-5) are AURORA KA-3653;ANILINOACETIC ACID;H-PHENYLGLY-OH;AKOS B003332;RARECHEM AL BO 1139;N-PHENYLGLYCIN;N-PHENYLGLYCINE;N-PHENYL-GLY-OH
The molecular structure of N-phenylglycine(103-01-5):
N-phenylglycine(103-01-5) has a melting point of 121-123 °C(lit.).
The chemical synonyms of N-phenylglycine(103-01-5) are AURORA KA-3653;ANILINOACETIC ACID;H-PHENYLGLY-OH;AKOS B003332;RARECHEM AL BO 1139;N-PHENYLGLYCIN;N-PHENYLGLYCINE;N-PHENYL-GLY-OH
The molecular structure of N-phenylglycine(103-01-5):
Toxicity Data With Reference
RTECS#: CAS# 103-01-5: None listed
LD50/LC50: RTECS: Not available.
Carcinogenicity: N-PHENYLGLYCINE, 93%(TLC) - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.
LD50/LC50: RTECS: Not available.
Carcinogenicity: N-PHENYLGLYCINE, 93%(TLC) - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.
Safety Profile
Safety Statements 22-24/25
WGK Germany 3
HS Code 29224995
WGK Germany 3
HS Code 29224995
Specification
Chemical Stability: Stable under normal temperatures and pressures.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, irritating and toxic fumes and gases, carbon dioxide, nitrogen.
Hazardous Polymerization Has not been reported.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, irritating and toxic fumes and gases, carbon dioxide, nitrogen.
Hazardous Polymerization Has not been reported.