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103-80-0

Basic Information
CAS No.: 103-80-0
Name: phenylacetyl chloride
Article Data: 166
Molecular Structure:
Molecular Structure of 103-80-0 (phenylacetyl chloride)
Formula: C8H7ClO
Molecular Weight: 154.596
Synonyms: Benzeneacetyl chloride;Acetylchloride, phenyl- (6CI,7CI,8CI);2-Phenylacetyl chloride;2-Phenylethanoylchloride;Phenacetyl chloride;Phenylacetic acid chloride;Phenylaceticchloride;a-Phenylacetyl chloride;
EINECS: 203-146-5
Density: 1.16 g/cm3
Melting Point: 91oC
Boiling Point: 218.7 °C at 760 mmHg
Flash Point: 90 °C
Appearance: Colourless liquid
Hazard Symbols: CorrosiveC
Risk Codes: 34-37-14
Safety: 26-36/37/39-45-25-27
Transport Information: UN 2577 8/PG 2
PSA: 17.07000
LogP: 1.99450
Synthetic route
103-82-2

phenylacetic acid

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
With thionyl chloride In dichloromethane100%
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 23℃;100%
With thionyl chloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere;100%
383865-57-4

4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine

A

N-(4-Methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-2-phenyl-acetamide

B

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
A 37%
B n/a
103-82-2

phenylacetic acid

79-37-8

oxalyl dichloride

103-80-0

phenylacetyl chloride

79-37-8

oxalyl dichloride

114-70-5

sodium phenylacetate

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
With benzene
937611-56-8

4-chloro-1,3,4-triphenyl-butan-2-one

A

588-59-0

stilbene

B

103-80-0

phenylacetyl chloride

5437-84-3

phenyl-acetic acid hydrazide; hydrochloride

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
With Nitroethane; chlorine
114-70-5

sodium phenylacetate

A

1555-80-2

phenylacetic anhydride

B

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride
79-37-8

oxalyl dichloride

108-88-3

toluene

94-36-0

dibenzoyl peroxide

103-80-0

phenylacetyl chloride

103-82-2

phenylacetic acid

79-37-8

oxalyl dichloride

71-43-2

benzene

A

1555-80-2

phenylacetic anhydride

B

103-80-0

phenylacetyl chloride

140-29-4

phenylacetonitrile

103-80-0

phenylacetyl chloride

Conditions
ConditionsYield
With thionyl chloride; sulfuric acid Multistep reaction;
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  • Phenylacetylchloride

  • Casno:

    103-80-0

    Phenylacetylchloride

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    PhenylacetylchlorideAppearance:White fine powder Storage:Kept in a cool,dry and ventilated place Package:Foil bags or Customized Application:Meets the requirements Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF e

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  • Phenylacetyl Chloride

  • Casno:

    103-80-0

    Phenylacetyl Chloride

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  • Amadis Chemical offer CAS#103-80-0;CAT#A800808

  • Casno:

    103-80-0

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  • 103-80-0             C8H7ClO                 Phenylacetyl chloride

  • Casno:

    103-80-0

    103-80-0 C8H7ClO Phenylacetyl chloride

    Min.Order: 10 Gram

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    Phenylacetyl chloride Basic information Product Name: Phenylacetyl chloride Synonyms: Acetyl chloride, phenyl-;alpha-Phenylacetyl chloride;alpha-Toluyl chloride

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  • Phenylacetyl Chloride/99.5%

  • Casno:

    103-80-0

    Phenylacetyl Chloride/99.5%

    Min.Order: 1 Kilogram

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  • Phenylacetyl chloride

  • Casno:

    103-80-0

    Phenylacetyl chloride

    Min.Order: 1 Kilogram

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Specification

The Phenylacetyl chloride with CAS registry number of 103-80-0 is also known as Phenylacetic acid chloride. The IUPAC name is 2-Phenylacetyl chloride. It belongs to product categories of Pharmaceutical Intermediates; Acid Halides; Carbonyl Compounds; Organic Building Blocks. Its EINECS registry number is 203-146-5. In addition, the formula is C8H7ClO and the molecular weight is 154.60. This chemical is a colourless liquid that soluble in water and ether. It may destroy living tissue on contact and should be sealed in ventilated, cool, dry place away from oxidants, alkali, alcohols and water. What's more, this chemical is used as intermediates for pharmaceuticals, pesticides, spices and organic synthesis.

Physical properties about Phenylacetyl chloride are: (1)ACD/LogP: 1.628; (2)ACD/LogD (pH 5.5): 1.63; (3)ACD/LogD (pH 7.4): 1.63; (4)ACD/BCF (pH 5.5): 10.17; (5)ACD/BCF (pH 7.4): 10.17; (6)ACD/KOC (pH 5.5): 183.07; (7)ACD/KOC (pH 7.4): 183.07; (8)#H bond acceptors: 1; (9)#Freely Rotating Bonds: 2; (10)Index of Refraction: 1.535; (11)Molar Refractivity: 40.681 cm3; (12)Molar Volume: 130.755 cm3; (13)Polarizability: 16.127 10-24cm3; (14)Surface Tension: 39.2970008850098 dyne/cm; (15)Density: 1.182 g/cm3; (16)Flash Point: 89.971 °C; (17)Enthalpy of Vaporization: 45.51 kJ/mol; (18)Boiling Point: 218.704 °C at 760 mmHg; (19)Vapour Pressure: 0.123999997973442 mmHg at 25°C

Preparation of Phenylacetyl chloride: it is prepared by reaction of benzeneacetic acid with thionyl chloride. The reaction releases sulfur dioxide and hydrogen chloride gas at room temperature. When reaction is complete, the reaction mixture is heated to 30-40 °C for 25 hours and benzene is added. After steaming volatile matter, product is obtained by collecting distillate at 55-57 °C (0.133kPa). The yield is about 80-85%.

Uses of Phenylacetyl chloride: it is used to produce 1,2-diphenyl-ethanone by reaction with iodobenzene. The reaction occurs with reagent NBu4BF4, catalyst NiBr2bpy and solvent acetonitrile with ambient temperature. The yield is about 35%.

Phenylacetyl chloride is used to produce 1,2-diphenyl-ethanone by reaction with iodobenzene.

When you are using this chemical, please be cautious about it. As a chemical, it is irritating to respiratory system and reacts violently with water. It can cause burns. During using it, wear suitable protective clothing, gloves and eye/face protection. Avoid contact with eyes. After using it, take off immediately all contaminated clothing. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. If accident happens or you feel unwell seek medical advice immediately.

You can still convert the following datas into molecular structure:
1. Canonical SMILES: C1=CC=C(C=C1)CC(=O)Cl
2. InChI: InChI=1S/C8H7ClO/c9-8(10)6-7-4-2-1-3-5-7/h1-5H,6H2
3. InChIKey: VMZCDNSFRSVYKQ-UHFFFAOYSA-N

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